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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/10/20 21:23 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AAD0068-EPA 7471A <br /> LCS Dup(A A D0068-BSD1) Prepared&Analyzed:04/10/20 <br /> Mercury 0.214 0.016 mg/kg 0.200 107 80-120 2.21 20 <br /> Matrix Spike(AAD0068-MS1) Source:2004042-01 Prepared&Analyzed:04/10/20 <br /> Mercury 0.225 0.016 mg/kg 0.200 ND 112 75-125 <br /> Matrix Spike Dup(AAD0068-MSD1) Source:2004042-01 Prepared&Analyzed:04/10/20 <br /> Mercury 0.221 0.016 mg/kg 0.200 ND 110 75-125 1.80 20 <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page II of 19 <br />