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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/10/20 21:23 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AAD0069-EPA 7470A <br /> Matrix Spike(AAD0069-MS1) Source:2004047-01 Prepared&Analyzed:04/10/20 <br /> Mercury 0.178 0.0160 mg/L 0.200 ND 89.2 75-125 <br /> Matrix Spike Dup(AAD0069-MSD1) Source:2004047-01 Prepared&Analyzed:04/10/20 <br /> Mercury 0.170 0.0160 mg/L 0.200 ND 85.2 75-125 4.59 20 <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 15 of 19 <br />