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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/10/20 21:23 <br /> Notes and Definitions <br /> QM-01 The spike recovery for this QC sample is outside of established control limits due to sample matrix interference. <br /> QB-01 The method blank contains analyte at a concentration above the MRL;however,concentration is less than 10%of the <br /> sample result,which is negligible according to method criteria. <br /> ND Analyte not detected at reporting limit. <br /> NR Not reported <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 19 of 19 <br />