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QC Sample Results <br /> Client: Antea USA Inc . Job ID : 440-246095- 1 <br /> Project/Site : ARCO 7049 , Lodi <br /> Method : 826013/5035 - Volatile Organic Compounds ( GC/MS ) <br /> Lab Sample ID : MB 440 -558608/4 Client Sample ID : Method Blank <br /> Matrix : Solid Prep Type : Total /NA <br /> Analysis Batch : 558608 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> Benzene ND 0 .0020 0. 0010 mg/Kg 07/20/19 08 :34 1 <br /> Ethylbenzene ND 0 . 0020 0.0010 mg/Kg 07/20/19 08: 34 1 <br /> m , p-Xylene ND 0.0040 0 .0020 mg/Kg 07/20/19 08 :34 1 <br /> Methyl-t-Butyl Ether (MTBE) ND 0 .0050 0 .0010 mg/Kg 07/20/19 08 :34 1 <br /> Naphthalene ND 0 .0050 0. 0020 mg/Kg 07/20/19 08 : 34 1 <br /> o-Xylene ND 0 . 0020 0. 0010 mg/Kg 07/20/19 08 : 34 1 <br /> tert-Butyl alcohol (TBA) ND 0 . 10 0. 010 mg/Kg 07/20/19 08 :34 1 <br /> Toluene ND 0 .0020 0 .0010 mg/Kg 07/20/19 08 :34 1 <br /> Xylenes , Total ND 0 . 0040 0. 0020 mg/Kg 07/20/19 08 : 34 1 <br /> MB MB <br /> Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> 4-Bromofluorobenzene (Surr) 88 79 - 120 07/20/19 08:34 1 <br /> Dibromofluoromethane (Surr) 97 60 - 120 07/20/19 08:34 1 <br /> Toluene-d8 (Surr) 94 79 - 123 07/20/19 08:34 1 <br /> Lab Sample ID : LCS 440 -558608/8 Client Sample ID : Lab Control Sample <br /> Matrix : Solid Prep Type : Total/NA <br /> Analysis Batch : 558608 <br /> Spike LCS LCS % Rec. <br /> Analyte Added Result Qualifier Unit D % Rec Limits <br /> Benzene 0 .0200 0 . 0181 mg/Kg 90 65 - 120 <br /> Ethylbenzene 0.0200 0. 0188 mg/Kg 94 70 - 125 <br /> m , p-Xylene 0. 0200 0. 0188 mg/Kg 94 70 - 125 <br /> Methykt-Butyl Ether (MTBE) 0. 0200 0.0168 mg/Kg 84 60 - 140 <br /> Naphthalene 0.0200 0 .0226 mg/Kg 113 55 - 135 <br /> o-Xylene 0 .0200 0 .0191 mg/Kg 95 70 - 125 <br /> tert-Butyl alcohol (TBA) 0 .200 0.245 mg/Kg 123 70 - 135 <br /> Toluene 0 .0200 0. 0188 mg/Kg 94 70 - 125 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> 4-Bromofluorobenzene (Surr) 87 79 - 120 <br /> Dibromofluoromethane (Surr) 101 60 - 120 <br /> Toluene-d8 (Surr) 92 79 - 123 <br /> Lab Sample ID : LCSD 440 -558608/9 Client Sample ID : Lab Control Sample Dup <br /> Matrix : Solid Prep Type : Total /NA <br /> Analysis Batch : 558608 <br /> Spike LCSD LCSD % Rec. RPD <br /> Analyte Added Result Qualifier Unit D % Rec Limits RPD Limit <br /> Benzene 0. 0200 0 .0182 mg/Kg 91 65 - 120 1 20 <br /> Ethylbenzene 0.0200 0 . 0190 mg/Kg 95 70 - 125 1 20 <br /> m ,p-Xylene 0 .0200 0 . 0191 mg/Kg 95 70 - 125 1 20 <br /> Methykt-Butyl Ether (MTBE) 0 .0200 0. 0167 mg/Kg 84 60 - 140 0 25 <br /> Naphthalene 0 .0200 0. 0228 mg/Kg 114 55 - 135 1 25 <br /> o-Xylene 0 .0200 0. 0198 mg/Kg 99 70 - 125 4 20 <br /> tert-Butyl alcohol (TBA) 0. 200 0 .246 mg/Kg 123 70 - 135 0 20 <br /> Toluene 0. 0200 0 .0189 mg/Kg 94 70m125 1 20 <br /> Eurofins TestAmerica , Irvine <br /> Page 39 of 104 7/25/2019 <br />