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QC Sample Results Client : Antea USA Inc . Job ID : 440-246095- 1 Project/Site : ARCO 7049 , Lodi Method : 8270C SIM - Semivolatile Organic Compounds ( GC/MS SIM ) Lab Sample ID : 440 -246095 -1 MSD Client Sample ID : T4E-15_20190716 Matrix : Solid Prep Type : Total /NA Analysis Batch : 558411 Prep Batch : 558464 Sample Sample Spike MSD MSD % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits RPD Limit Acenaphthene ND 0. 0690 0. 0507 mg/Kg 74 10 - 150 3 39 Acenaphthylene ND 0 , 0690 0 .0509 mg/Kg 74 23 - 114 5 38 Anthracene ND 0 .0690 0 .0510 mg/Kg 74 10 - 150 4 40 Benzo[a]anthracene ND 0. 0690 0. 0541 mg/Kg 78 10m150 5 40 Benzo[a]pyrene ND 0. 0690 0.0528 mg/Kg 77 10 - 150 7 40 0 Benzo[b]fluoranthene ND 0 .0690 0 .0547 mg/Kg 79 10 - 150 3 40 Benzo[g , h , i]perylene ND 0 .0690 0.0487 mg/Kg 71 10 - 143 6 40 Benzo[k]fluoranthene ND 0. 0690 0. 0502 mg/Kg 73 10 - 150 7 40 Chrysene ND 0 . 0690 0. 0524 mg/Kg 76 10 - 150 3 40 Dibenz(a , h)anthracene ND 0 , 0690 0 .0510 mg/Kg 74 10 - 127 8 40 Fluoranthene ND 0 .0690 0 .0529 mg/Kg 77 10 - 150 6 40 Fluorene ND 0 . 0690 0. 0515 mg/Kg 75 10 - 150 4 40 Indeno[1 ,2 ,3-cd] pyrene ND 0. 0690 0. 0518 mg/Kg 75 10 - 138 6 40 Naphthalene ND 0 .0690 0.0470 mg/Kg 68 10 - 150 7 40 Phenanthrene ND 0 .0690 0 .0508 mg/Kg 74 10 - 150 5 40 Pyrene ND 0 .0690 0.0527 mg/Kg 76 10 - 150 7 40 MSD MSD Surrogate %Recovery Qualifier Limits 2-Fluorobiphenyl (Surr) 72 29 - 129 LNitrobenzene-d5 69 29 - 126 Terphenyl-d14 80 28 - 145 Lab Sample ID : MB 440 -558534/1 -A Client Sample ID : Method Blank Matrix : Solid Prep Type : Total/NA Analysis Batch : 558613 Prep Batch : 558534 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 .030 0.0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Acenaphthylene ND 0 .030 0. 0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Anthracene ND 0 .030 0. 0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Benzo[a]anthracene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Benzo[a]pyrene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Benzo[b]fluoranthene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Benzo[g , h ,i]perylene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07:47 1 Benzo[k]fluoranthene ND 0 .030 0.0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Chrysene ND 0 .030 0.0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Dibenz(a , h)anthracene ND 0.030 0. 0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Fluoranthene ND 0 .030 0. 0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Fluorene ND 0 .030 0. 0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Indeno[1 ,2 ,3-cd]pyrene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Naphthalene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Phenanthrene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 Pyrene ND 0 .030 0 .0040 mg/Kg 07/19/19 16 : 19 07/20/19 07 :47 1 MB MB Surrogate %Recovery Qualifier Limits Prepared Analyzed DYFac 2-Fluorobiphenyl (Surr) 81 29 - 129 07/19/19 16: 19 07/20/19 07:47 1 Nitrobenzene-d5 70 29 - 126 07/19/19 16: 19 07/20/19 07:47 1 Terphenyl-d14 90 28 - 145 07/19/19 16: 19 07/20/19 07:47 1 Eurofins TestAmerica , Irvine Page 43 of 104 7/25/2019 i E