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QC Sample Results <br /> Client: Antea USA Inc . Job ID : 440-246095- 1 <br /> Project/Site : ARCO 7049 , Lodi <br /> -- - - - ---- — <br /> Method : 80158 - Diesel Range Organics ( DRO ) ( GC ) ( Continued ) <br /> Lab Sample ID : 440446095 -1 MSD Client Sample ID : T4E -15_20190716 <br /> Matrix : Solid Prep Type : Total/NA <br /> Analysis Batch : 558413 Prep Batch : 558465 <br /> Sample Sample Spike MSD MSD % Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit <br /> C10-C28 2.7 J , DX 70. 9 66 .2 mg/Kg 90 40 - 120 3 30 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> n-Octacosane 88 40 - 140 <br /> Lab Sample ID : MB 440 -558967/1 -A Client Sample ID : Method Blank <br /> Matrix : Solid Prep Type : Total/NA <br /> Analysis Batch : 559028 Prep Batch : 558967 <br /> MB MB <br /> Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac <br /> DRO (C13-C22) ND 5 . 0 2 .5 mg/Kg 07/23/19 06 : 19 07/23/19 11 :45 1 <br /> ORO (C23-C40) ND 5 . 0 2 . 5 mg/Kg 07/23/19 06: 19 07/23/19 11 :45 1 <br /> MB MB <br /> j Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac <br /> Ln-Octacosane 69 40 - 140 -6712311906: 19 07/23/19 11 :45 1 <br /> [ Lab Sample ID : LCS 440 -558967/2 -A Client Sample ID : Lab Control Sample <br /> Matrix : Solid Prep Type : Total /NA <br /> Analysis Batch : 559028 Prep Batch : 558967 <br /> Spike LCS LCS % Rec. <br /> Analyte Added Result Qualifier Unit D % Rec Limits <br /> C10-C28 66 .7 62 . 9 mg/Kg 94 45 - 115 <br /> LCS LCS <br /> Surrogate %Recovery Qualifier Limits <br /> n-Octacosane 73 40 - 140 <br /> r Lab Sample ID : 440 -246329 -M -1 -B MS Client Sample ID : Matrix Spike <br /> Matrix : Solid Prep Type : Total/NA <br /> Analysis Batch : 559028 Prep Batch : 558967 <br /> Sample Sample Spike MS MS % Rec. <br /> Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits <br /> C10-C28 4 .3 J , DX 64. 7 58 .7 mg/Kg 84 40 - 120 <br /> MS MS <br /> Surrogate %Recovery Qualifier Limits <br /> Ln-Octacosane 70 40 - 140 <br /> Lab Sample ID : 440 -246329 -M - 1 -C MSD Client Sample ID : Matrix Spike Duplicate <br /> Matrix : Solid Prep Type : Total /NA <br /> Analysis Batch : 559028 Prep Batch : 558967 <br /> Sample Sample Spike MSD MSD % Rec. RPD <br /> Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit <br /> C10-C28 4 .3 J , DX 65.6 57 .9 mg/Kg 82 40 . 120 2 30 <br /> MSD MSD <br /> Surrogate %Recovery Qualifier Limits <br /> n-Octacosane 73 40 - 140 <br /> Eurofins TestAmerica , Irvine <br /> Page 49 of 104 7/25/2019 <br /> i <br /> i <br />