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GC / MS SEMI VOA BATCH WORKSHEET <br /> Lab Name : Eurofins TestAmerica , Irvine Job No . : 440 - 246095 - 1 <br /> SDG No . : <br /> Batch Number : 558534 Batch Start Date : 07 / 19 / 19 16 : 19 Batch Analyst : Hamblin , Alyssa J <br /> Batch Method : 3546 Batch End Date : <br /> Lab Sample ID Client Sample ID Method Chain Basis InitialAmount FinalAmount SVWLE 00014 SVWSE 00021 AnalysisComment <br /> MB 440 - 558534 / 1 3546 , 8270C 15 . 00 g 1 mL 0 . 5 mL 3546 8270 SIM <br /> SIM PAH <br /> LCS 3546 , 8270C 15 . 00 g 1 mL 0 . 5 mL 0 . 5 mL <br /> 440 - 558534 / 2 SIM <br /> 440 - 246095 -G- 21 PL2 - 2_20190716 3546 , 8270C T 15 . 12 g 1 mL 0 . 5 mL moist brown <br /> SIM sand <br /> Batch Notes <br /> Balance ID 61 <br /> Batch Comment 40 mL VOA vial lot 4B237533 - 2 - 19170 <br /> Blank Matrix ID OTTAWA SAND 5455122 <br /> Analyst ID - Concentration AH EC <br /> Concentration 1 Corrected Temperature 40 Degrees C <br /> Equipment ID - Concentration 1 XcelVap 03 <br /> Analyst ID - Extraction AH EC <br /> Filter ID 19 - 025 <br /> Method/ Fraction 3546 8270C SIM PAH <br /> Microwave Oven ID 1 <br /> Na2SO4 ID 5680995 <br /> Pipette / Syringe / Dispenser ID 0 . 50 mL ( 060319500A ) <br /> Prep Solvent ID McC12 ( 5679855 ) Acetone ( 5611952 ) <br /> Analyst ID - Spike Analyst AH <br /> Sufficient Volume for Batch QC Y <br /> Concentration 1 Uncorrected Temperature 40 Degrees C <br /> Vial Lot Number 19033719 <br /> Basis Basis Description <br /> T Total / NA <br /> The pound sign ( # ) in the amount added field denotes that the reagent was used undiluted . All calculations are performed using the stated concentration for <br /> this reagent . <br /> 8270C SIM Page 1 of 1 <br /> Page 84 of 104 7/25/2019 <br />