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Client Sample Results Job ID : 440-246101 - 1 Client: Antea USA Inc . Project/Site : ARCO 7049 , Lodi - Client Sample ID : StockpilelA_20190716 Lab Sample ID : 440 -246101 -2 Matrix : Solid Date Collected : 07/ 16/19 14 : 55 Percent Solids : 91 . 6 Date Received : 07/18/ 19 07 : 30 - - - Method : 82608/5035 - Volatile Organic Compounds (GC/MS ) [Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 0 .0015 0.00074 mg/Kg 07/18/19 08: 00 07/19/19 10 :43 1 Benzene 07/18/19 08: 00 07/19/19 10 :43 1 3 Ethylbenzene ND 0 .0015 0 .00074 mg/Kg ND 0 .0030 0. 0015 mg/Kg 07/18/19 08: 00 07/19/19 10 :43 1 Methylrn ,pwXyteBu 07/18/19 08: 00 07/19/19 10 :43 1 Methyl-t-Butyl Ether (MTBE) ND 0 . 0037 0. 00074 mg/Kg ND 0 . 0037 0. 0015 mg/Kg 07/18/19 08 : 00 07/19/19 10 :43 1 Naphthalene 07/18/19 08 :00 07/19/19 10 :43 1 o-Xylene ND 0 .0015 0.00074 mg/Kg tert-Butyl alcohol (TBA) ND 0 .074 0.0074 mg/Kg 07/18/19 08: 00 07/19/19 10 :43 1 ND 0 .0015 0.00074 mg/Kg � 07/18/19 08:00 07/19/19 10:43 1 Toluene Xylenes, Total ND 0 . 0030 0. 0015 mg/Kg 07/18/19 08 :00 07/19/19 10 :43 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4 Bromofluorobenzene (Burr) 91 79 - 120 07/18/19 08:00 07/19/19 10:43 1 Dibromofluoromethane (Surr) 99 60 - 120 07/18/19 08:00 07/19/19 10:43 1 L07/18/19 08:00 07/19/19 10:43 1 Toluene-d8 (Surr) 98 79 - 123 Method : 8270C SIM - Semivolatile Organic Compounds (GC/MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac ND 0 . 032 0 . 0043 mg/Kg 0 07/18/1913:35 07/19/1915: 37 1 Acenaphthene 07/18/1913: 35 07/19/1915 : 37 1 Acenaphthylene ND 0 . 032 0 .0043 mg/Kg ND 0 .032 0 .0043 mg/Kg 0 07/18/1913: 35 07/19/1915 :37 1 Anthracene 07/18/1913: 35 07/19/1915 :37 1 Benzo[a]anthracene ND 0 .032 0 .0043 mg/Kg ND 0 .032 0. 0043 mg/Kg 07/18/1913 : 35 07/19/1915 :37 1 Benzo[a]pyrene 07/18/1913 : 35 07/19/1915 :37 1 Benzo[b]fluoranthene ND 0 .032 0. 0043 mg/Kg Benzo[g ,h ,i]perylene ND 0 .032 0.0043 mg/Kg 07/18/1913 : 35 07/19/1915 :37 1 ND 0 .032 0. 0043 mg/Kg � 07/18/1913 :35 07/19/1915 :37 1 Benzo[k]fluoranthene 07/18/1913 : 35 07/19/1915 :37 1 Chrysene ND 0 . 032 0 .0043 mg/Kg ND 0 . 032 0 .0043 mg/Kg 07/18/1913: 35 07/19/1915 : 37 1 Dibenz(a , h)anthracene 07/18/1913: 35 07/19/1915 :37 1 Fluoranthene ND 0 .032 0 .0043 mg/Kg ND 0 .032 0 .0043 mg/Kg � 07/18/1913: 35 07/19/1915 :37 1 Fluorene 07/18/1913 : 35 07/19/1915 :37 1 lndeno[1 ,2 ,3-cd] pyrene ND 0 .032 0.0043 mg/Kg ND 0 .032 0. 0043 mg/Kg 07/18/1913 : 35 07/19/1915 :37 1 Naphthalene 07/18/1913 :35 07/19/1915 : 37 1 Phenanthrene ND 0 .032 0. 0043 mg/Kg 0 .032 0 . 0043 mg/Kg � 07/18/1913: 35 07/19/1915 :37 1 Pyrene ND Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 56 29 - 129 2 Fluorobiphenyl (Surr) 07/18/19 13:35 07/19/19 15:37 1 Nitrobenzene-d5nyl 55 29 - 126 07/18/19 13:35 07/19/19 15:37 1 07/18/1913:35 07/19/1915:37 1 LTerphenyl-d14 62 28 - 145 ( Method : 8015B/5035 - Gasoline Range Organics (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed DiI Fac i GRO (C4-C12) 0 . 12 J , DX 0. 33 0 . 12 mg/Kg 07/18/19 12 : 30 07/20/19 20:08 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 91 '65 - 140 -6-7'11811912. 30 07/20/19 20:08 1 FMethod : 80158 - Diesel Range Organics ( DRO ) (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C13-C22) ND 5 .4 2 .7 mg/Kg 07/18/19 13 : 32 07/19/19 0027 1 ORO (C23-C40) 10 5 .4 2 .7 mg/Kg 07/18/19 13 :32 07/19/19 00 :27 1 Eurofins TestAmerica , Irvine Page 6 of 38 8/ 12/2019 ( Rev. 1 )