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Surrogate Summary <br /> Job ID : 440-246101 - 1 <br /> Client: Antea USA Inc . <br /> Project/Site : ARCO 7049 , Lodi — <br /> Method : 826013/5035 as Volatile Organic Compounds ( GC/MS ) Prep Type : Total/ NA <br /> Matrix : Solid <br /> Percent Surrogate Recovery (Acceptance Limits) <br /> BFB DBFM TOL <br /> Lab Sample ID Client Sample ID (79A20) (60=120) (79-123) <br /> 1440m246101 -2 StockpilelA_20190716 91 99 98 <br /> 440-246101 -3 StockpilelB_20190716 89 100 97 <br /> 440-246101 -4 Trip Blanks 92 100 99 <br /> LCS 440-558387/5 Lab Control Sample 91 100 95 <br /> LCSD 440-558387/6 Lab Control Sample Dup 90 98 98 <br /> MB 440-558387/4 Method Blank 95 92 103 <br /> Surrogate Legend <br /> BFB = 4-Bromofluorobenzene (Burr) <br /> DBFM = Dibromofluoromethane (Surr) <br /> L TOL = Toluene-0 (Surr) - - — <br /> Method : 8270C SIM - Semivolatile Organic Compounds ( GC /MS SIM ) Prep Type : Total/NA <br /> Matrix : Solid_ -- -- -- <br /> Percent Surrogate Recovery (Acceptance Limits) <br /> FBP NBZ TPHL <br /> Lab Sample ID Client Sample ID (29-129) (29-126) (28-145) <br /> 440-246100-H 8-D MS Matrix Spike 78 75 89 <br /> 440-2461 00-1-1-&E MSD Matrix Spike Duplicate 80 75 87 <br /> 440 246101 -2 StockpilelA_20190716 56 55 62 <br /> 440-246101 -3 StockpilelB 20190716 76 74 82 <br /> LCS 440-558277/2-A Lab Control Sample 82 84 93 <br /> MB 440-558277/1 -A Method Blank 82 85 97 <br /> Surrogate Legend <br /> FBP = 2-Fluorobiphenyl (Surr) <br /> NBZ = Nitrobenzene-d5 <br /> L TPHL = Terphenyl-d14 — _— <br /> Method : 801513/ 5035 - Gasoline Range Organics ( GC ) Pre Type : Total/ NA <br /> Matrix : Solid _- - — — p Y ---- <br /> r- Percent Surrogate Recovery (Acceptance Limits) <br /> I BFB1 <br /> Lab Sample ID Client Sample ID (65-140) <br /> 440-246101 -2 Stockpile 1 A_201 90716 91 <br /> 440-246101 -3 Stockpile 1 B_201 90716 93 <br /> 440-246101 -4 Trip Blanks 92 <br /> LCS 440-558624/6 Lab Control Sample 96 <br /> LCSD 440-558624/7 Lab Control Sample Dup 97 <br /> MB 440-558624/8 Method Blank 88 <br /> Surrogate Legend <br /> LBFB = 4-Bromofluorobenzene (Surr) <br /> Eurofins TestArrerica , Irvine <br /> Page 9 of 38 8/ 12/2019 ( Rev . 1 ) <br />