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Client: Antea USA Inc . QC Sample Results Job ID : 440-246101 - 1 Project/Site : ARCO 7049 , Lodi Method : 8270C SIM - Semivolatile Organic Compounds ( GC/ MS SIM ) ( Continued ) ----- Lab Sample ID : LCS 440 -558277/2 -A Client Sample ID : Lab Control Sample Matrix : Solid Prep Type : Total/NA Prep Batch : 558277 Analysis Batch : 558411 Spike LCS LCS % Rec . Analyte Added Result Qualifier Unit D % Rec Limits Fluoranthene 0. 0667 0.0555 mg/Kg 83 59 - 128 Fluorene 0.0667 0. 0547 mg/Kg 82 59 - 134 Indeno[1 ,2 ,3-cdjpyrene 0.0667 0 .0552 mg/Kg 83 51 - 120 Naphthalene 0 .0667 0 .0520 mg/Kg 78 58 - 120 Phenanthrene 0 .0667 0 .0540 mg/Kg 81 58 - 120 Pyrene 0 .0667 0.0552 mg/Kg 83 59 - 127 LCS LCS Surrogate %Recovery Qualifier Limits Fluorobiphenyl (Surr) 82 29 - 129 2- Nitrobenzene-d5 84 29 - 126 TerphenyPd 14 93 28 - 145 Lab Sample ID : 440 -246100 -H -8 - D MS Client Sample ID : Matrix Spike Prep Type : Total / NA Matrix : Solid Prep Batch : 558277 Analysis Batch : 558411 Sample Sample Spike MS MS % Rec . Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits Acenaphthene ND 0.0746 0 .0573 mg/Kg 77 10 - 150 Acenaphthylene ND 0 .0746 0 .0489 mg/Kg 66 23 - 114 Anthracene ND 0.0746 0. 0580 mg/Kg 78 10 - 150 Benzo[a]anthracene ND 0.0746 0.0625 mg/Kg 84 10 - 150 Benzo[a] pyrene ND 0 .0746 0 .0608 mg/Kg 81 10 - 150 Benzo[b]fluoranthene ND 0 .0746 0.0643 mg/Kg 86 10 - 150 Benzo[g , h ,i]perylene ND 0. 0746 0. 0625 mg/Kg 3� 84 10 - 143 Benzo[k]fluoranthene ND 0.0746 0 .0592 mg/Kg 79 10 ,s150 Chrysene ND 0 .0746 0 .0607 mg/Kg 81 10 - 150 Dibenz(a , h)anthracene ND 0. 0746 0. 0610 mg/Kg 3� 82 10 - 127 Fluoranthene ND 0.0746 0 .0619 mg/Kg 83 10 - 150 Fluorene ND 0 .0746 0 .0599 mg/Kg 3� 80 10 - 150 Indeno[1 , 2 ,3-cd] pyrene ND 0 .0746 0. 0629 mg/Kg 84 10 - 138 Naphthalene ND 0. 0746 0.0561 mg/Kg 75 10 - 150 Phenanthrene ND 0 .0746 0 .0592 mg/Kg 3� 79 10 - 150 Pyrene ND 0 .0746 0. 0615 mg/Kg 82 10 - 150 MS MS Surrogate %Recovery Qualifier Limits 2-Fluorobiphenyl (Surr) 78 29 - 129 Nitrobenzene-d5 75 29 - 126 L Terphenyl-d14 89 28 - 145 Lab Sample ID : 440 -246100 -H -8 -E MSD Client Sample ID : Matrix Spike Duplicate Matrix : Solid Prep Type : Total/NA Analysis Batch : 558411 Prep Batch : 558277 Sample Sample Spike MSD MSD % Rec. RPD Analyte Result Qualifier Added Result Qualifier Unit D % Rec Limits RPD Limit Acenaphthene ND 0 .0751 0 .0606 mg/Kg 81 10 - 150 6 39 Acenaphthylene ND 0 .0751 0.0546 mg/Kg 73 23 - 114 11 38 Anthracene ND 0. 0751 0 . 0605 mg/Kg 81 10 - 150 4 40 Benzo[a]anthracene ND 0 .0751 0 .0658 mg/Kg 88 10 - 150 5 40 Eurofins TestAmerica , Irvine Page 13 of 38 8/ 12/2019 ( Rev . 1 )