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Client Sample Results Client: Antea USA Inc . Job ID : 440-246095- 1 Project/Site : ARCO 7049 , Lodi Client Sample ID : T4E - 15_20190716 Lab Sample ID : 440 -246095 - 1 Date Collected : 07 /16 /19 10 : 50 Matrix : Solid Date Received : 07/18/19 07 : 30 Percent Solids : 94 . 0 Method : 826013/5035 - Volatile Organic Compounds ( GC/MS ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Benzene ND 0 .0022 0.0011 mg/Kg 07/18/19 08: 00 07/20/19 09 :46 1 Ethylbenzene ND 0 . 0022 0 .0011 mg/Kg 07/18/19 08 : 00 07/20/19 09 :46 1 m , p-Xylene ND 0 .0044 0 .0022 mg/Kg 07/18/19 08 : 00 07/20/19 09 :46 1 Methyl-t-Butyl Ether (MTBE) ND 0 .0055 0. 0011 mg/Kg 07/18/19 08: 00 07/20/19 09 :46 1 Naphthalene ND 0 . 0055 0 .0022 mg/Kg 0 07/18/19 08: 00 07/20/19 09 :46 1 o-Xylene ND 0 . 0022 0 .0011 mg/Kg 07/18/19 08 :00 07/20/19 09 :46 1 tert- Butyl alcohol (TBA) ND 0. 11 0.011 mg/Kg 07/18/19 08: 00 07/20/19 09 :46 1 Toluene ND 0 .0022 0 .0011 mg/Kg 07/18/19 08 : 00 07/20/19 09 :46 1 Xylenes , Total ND 0 .0044 0 .0022 mg/Kg 07/18/19 08 :00 07/20/19 09 :46 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 92 79 - 120 07/18/19 08:00 07/20/19 09:46 1 Dibromofluoromethane (Surr) 103 60 - 120 07/18/19 08:00 07/20/19 09:46 1 Toluene-d8 (Surr) 97 79 - 123 07/18/19 08:00 07/20/19 09:46 1 Method : 8270C SIM - Semivolatile Organic Compounds (GC /MS SIM ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Acenaphthene ND 0 .031 0.0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Acenaphthylene ND 0 . 031 0. 0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Anthracene ND 0 .031 0. 0042 mg/Kg 07/19/1911 : 23 07/19/1919 : 28 1 Benzo[a]anthracene ND 0 .031 0 .0042 mg/Kg 0 07/19/1911 : 23 07/19/1919 :28 1 Benzo [a]pyrene ND 0 .031 0 .0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Benzo[b]fluoranthene ND 0 . 031 0. 0042 mg/Kg 0 07/19/1911 :23 07/19/1919 :28 1 Benzo[g , h , i]perylene ND 0 . 031 0.0042 mg/Kg 07/19/1911 : 23 07/19/1919 :28 1 Benzo[k]fluoranthene ND 0 .031 0 .0042 mg/Kg 3� 07/19/1911 :23 07/19/1919 :28 1 Chrysene ND 0 .031 0 .0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Dibenz(a , h)anthracene ND 0 .031 0.0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Fluoranthene ND 0 . 031 0. 0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Fluorene ND 0 .031 0. 0042 mg/Kg 07/19/1911 : 23 07/19/1919 :28 1 Indeno[1 ,2 , 3-cd]pyrene ND 0 .031 0 .0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Naphthalene NO 0 .031 0 .0042 mg/Kg 0 07/19/1911 :23 07/19/1919 :28 1 Phenanthrene ND 0 . 031 0.0042 mg/Kg # 07/19/1911 :23 07/19/1919 :28 1 Pyrene ND 0 . 031 0. 0042 mg/Kg 07/19/1911 :23 07/19/1919 :28 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 2-Fluorobiphenyl (Surr) 84 29 - 129 07/19/19 11 :23 07/19/19 19:28 1 Nitrobenzene-d5 81 29 - 126 07/19/19 11 :23 07/19/19 19:28 1 Terphenyl-d14 93 28 - 145 07/19/19 11 :23 07/19/19 19:28 1 Method : 8015B/5035 - Gasoline Range Organics (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac GRO (C4-C12) ND 0 .44 0. 16 mg/Kg 07/18/19 09 :00 07/20/19 14 :07 1 Surrogate %Recovery Qualifier Limits Prepared Analyzed Dil Fac 4-Bromofluorobenzene (Surr) 118 65 - 140 07/18/19 09:00 07/20/19 14:07 1 Method : 80158 - Diesel Range Organics ( DRO) (GC ) Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac DRO (C13-C22) ND 5.3 2 .6 mg/Kg 0 07/19/19 11 :25 07/19/19 23 : 31 1 ORO (C23-C40) 4 .3 J , DX MB 5 .3 2 .6 mg/Kg 3� 07/19/19 11 :25 07/19/19 23 : 31 1 Eurofins TestAmerica , Irvine Page 9 of 104 7/25/2019 i I