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Case Narrative <br /> Client: Buckeye Terminal LLC TestAmerica Job ID: 720-69707-1 <br /> Project/Site: Stockton Grinder Dust Chop Saw <br /> Job ID: 720-69707-1 <br /> Laboratory: TestAmerica Pleasanton <br /> Narrative I <br /> Receipt <br /> The sample was received on 1/13/2016 at 12:40 PM.The sample arrived in good condition, properly preserved and,where required,on <br /> ice. The temperature of the cooler at receipt was 4.3°C. <br /> Method 60108 <br /> The matrix spike/matrix spike duplicate(MS/MSD) recoveries and precision for preparation batch 720-195658 and analytical batch <br /> 720-195898 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated <br /> laboratory control sample/laboratory sample control duplicate(LCS/LCSD)precision was within acceptance limits. <br /> Sample Grinder/chop saw Dust(720-69707-1)was diluted due to the abundance of non-target analytes(Fe&Mn)and thus elevated <br /> reporting limits(RLs)are provided. <br /> No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br /> TestAmerica Pleasanton <br /> Page 4 of 16 1/20/2016 <br />