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Case Narrative <br /> Client: Buckeye Terminal LLC TestAmerica Job ID: 720-69915-1 <br /> Project/Site: Carbon <br /> Job ID: 720-69915-1 <br /> Laboratory: TestAmerica Pleasanton <br /> Narrative I <br /> Receipt <br /> The sample was received on 1/22/2016 at 11:15 AM.The sample arrived in good condition, properly preserved and,where required,on <br /> ice. The temperature of the cooler at receipt was 1.0°C. <br /> Receipt Exceptions <br /> The chain of custody includes extraction for TCLP Benzene, however an incorrect container was used thus such testing was eliminated <br /> from this login. <br /> Metals 6010B <br /> The matrix spike/matrix spike duplicate(MS/MSD)recoveries and precision for preparation batch 720-196285 and analytical batch <br /> 720-196482 were outside control limits. Sample matrix interference and/or non-homogeneity are suspected because the associated <br /> laboratory control sample/laboratory sample control duplicate(LCS/LCSD)precision was within acceptance limits. <br /> No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. <br /> TestAmerica Pleasanton <br /> Page 4 of 16 1/29/2016 <br />