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MAY2018 <br /> CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 <br /> Certificate #2480 HF.ALTY�g)F.I A?a-pMg7 <br /> Technicon Engineering Client Project ID: 180321 Method: EPA 5030/8260B <br /> 4539 N. Brawley #108 Lab Reference Number: 1805035 Instrument ID: VARIAN MS <br /> Fresno, CA 93722 Sample Description: Soil Prepared: 05-15-18 <br /> Attn: Steve Curra Analyzed: 05-15-18 <br /> Reported: 05-16-18 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VSMS-5158 DP <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> mg/Kg m /Ko mg/Kg %R <br /> COMPOUNDS <br /> t-Butyl Alcohol (t-BA) 0. 10 ND 3.0 82.0% 70-130 <br /> Methyl t-butyl ether MTBE 0.0050 NO 0. 10 92.0% 70-130 <br /> Diiso ro I ether DIPE 0.0050 ND 0. 10 99.2% 70-130 <br /> Ethyl t-Bu I ether ETBE 0.0050 ND 0.10 93.2% 70-130 <br /> t-Am I methyl ether TAME 0.0050 ND 0.10 96.4% 70-130 <br /> 1 ,2-Dichloroethane 1 ,2-DCA 0.0050 NO 0. 10 94.4/ 70-130 <br /> Ethylene dibromide EDB 0.0050 NO 0.10 95.6% 70-130 <br /> 1 ,1-Dichloroethene 111 ,DCE 0.0050 ND 0.10 91 .6% 70-130 <br /> Benzene 0.0050 ND 0. 10 89.6% 70-130 <br /> Trichloroethene (TCE) 0.0050 ND 0.10 96.0% 70-130 <br /> Toluene 0.0050 ND 0.10 116% 70-130 <br /> Chlorobenzene 0.0050 NO 0.10 1010/0 70-130 <br /> Surro ate: <br /> Dibromofluoromethane 0. 10 104% 0.40 1000 <br /> 70-130 <br /> 1 ,2-Dichloroethane-d4 0. 10 99.6% 0.40 95.2% 70-130 <br /> Toluene-d8 0.10 1 93.9% 0.40 103% 70-130 <br /> 4-Bromofluorobenzene 0.10 119% 0.40 1 108% 70-130 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> m /K %R %R <br /> COMPOUNDS <br /> t-But I Alcohol t-BA 3.0 95.6% 110% 60-130% 13.6% <br /> Meth I t-bu tether MTBE 0. 10 92.4% 102% 70-130% 9.33% <br /> Diiso ro tether DIPE 0.10 99.6% 100°°/u 70-130% 2.37% <br /> Eth I t-Bu I ether ETBE 0.10 84.0% •87.6% 70-130% 3.74% <br /> t-Am Imeth tether TAME 0.10 98.0% 100% 70-130% 2.40 <br /> 1 ,2-Dichloroethane 1 ,2-DCA 0.10 95.6% 100% 70-130% 4.72% <br /> Eth lene dibromide EDB 0.10 86.8°°/a 97.6% 70-130% 11 .6% <br /> 1 ,1 -Dichloroethene 1 ,1 ,DCE 0. 10 67.2% 92.0% 60-130% 5.22% <br /> Benzene 0.10 89.6% 94.4% 70-130% 5.11 % <br /> Trichloroethene (TCE) 0.10 118% 127% 70-130% 7.38% <br /> Toluene 0.10 98.8% 102% 70-130% 3.55% <br /> Chlorobenzene 0.10 92.0% 98.4% 70-130% 4.59% <br /> Surrogate: <br /> Dibromofluoromethane 0.40 99.5% 98.2% 70-130% 1 .32% <br /> 1 ,2-Dichloroethane-d4 0.40 103% 105% 70-130% 1 .63% <br /> Toluene-d8 1 0.40 96. 1 % 101 % 70-130% 4.87% <br /> 4-Bromofluorobenzene 0.40 1 6% 113% 70-130% 3.41 % <br /> APPROVED BY: <br /> James C. Phillips / a oratory Director or <br /> Clan J. Cone / Lab ratory Manager <br />