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McCampbell Analytical, Inc. 1534 Willow Pass Road,Pittsburg,CA 94565-1701 j ,f:j,bJ Web:www.mcca7pbeff.com E-mail:main@mccampbell.com "When Oualitv Counts" TI,-,h,... le hone:877-252-9262 Fax:925-252-9269 QC SUMMARY REPORT FOR E300.0 W.O.Sample Matrix: Soil QC Matrix: Soil BatchlD: 43538 WorkOrder: 0906008 EPA Method E300.0 Extraction CA Title 22 modified Spiked Sample ID: N/A Analyte Sample Spiked MS MSD MS-MSD LCS LCSD LCS-LCSD Acceptance Criteria(%) mg/kg mg/kg %Rec. %Rec. %RPD % Rec. % Rec. %RPD MS/MSD RPD LCS/LCSD RPD Chloride N/A 100 N/A N/A N/A 89.8 89.9 0.0181 N/A N/A 80- 120 20 Sulfate N/A 100 N/A N/A N/A 104 104 0 N/A N/A 80- 120 20 %SS: N/A 10 1 N/A I N/A N/A 95 1 95 0 N/A N/A 80- 120 20 All target compounds in the Method Blank of this extraction batch were ND less than the method RL with the following exceptions: NONE BATCH 43538 SUMMARY Lab ID Date Sampled Date Extracted Date Analyzed Lab ID Date Sampled Date Extracted Date Analyzed 0906008-001 A 06/01/09 10:45 AM 06/01/09 06/03/09 6:16 PM I 0906008-002A 06/01/09 11:26 AM 06/01/09 06/03/09 7:37 PM MS=Matrix Spike;MSD=Matrix Spike Duplicate;LCS=Laboratory Control Sample;LCSD=Laboratory Control Sample Duplicate;RPD=Relative Percent Deviation. %Recovery=100'(MS-Sample)/(Amount Spiked);RPD=100'(MS- MSD)/((MS+MSD)/2). MS/MSD spike recoveries and/or%RPD may fall outside of laboratory acceptance criteria due to one or more of the following reasons:a)the sample is inhomogenous AND contains significant concentrations of analyte relative to the amount spiked,or b)the spiked sample's matrix interferes with the spike recovery. N/A=not applicable to this method,or not enough sample to perform matrix spike and matrix spike duplicate. NR=analyte concentration in sample exceeds spike amount for soil matrix or exceeds 2x spike amount for water matrix or sample diluted due to high matrix or analyte content. DHS ELAP Certification 1644 QA/QC Officer