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819 Striker Avenue, Suite 8 <br />Sacramento, CA 95834 <br />(916)921-9600 <br />FAX (916) 921-0100 <br />www. seq uoialabs.con; <br />Kleinfelder - Stockton Project: Granite Bumpile <br />2825 East `-lyrtle Street Project Number: 20-1108-33 Reported: <br />Stockton CA, 95205 Project Manager: Doug Heard 08/15/01 17:24 <br />Semivolatile Organic Compounds by EPA Method 8270C - Quality Control <br />Sequoia Analytical - Walnut Creek <br />Reporting Spike Source %REC RPD <br />Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br />Batch 1H02022 - EPA 3550B Sonication <br />Blank (1H02022-BLK1) <br />Prepared: 08/02/01 Analyzed: 08/04/01 <br />Acenaphthene <br />ND <br />0.10 mg/kg <br />Acenaphthylene <br />ND <br />0.10 " <br />Anthracene <br />ND <br />0.10 " <br />Aniline <br />ND <br />0.10 - <br />Benzoic acid <br />ND <br />0.50 " <br />Benzo (a) anthracene <br />ND <br />0.10 " <br />Benzo (b) fluoranthene <br />ND <br />0.25 " <br />Benzo (k) fluoranthene <br />ND <br />0.25 " <br />Benzo (ghi) perylene <br />ND <br />0.10 " <br />Benzo[a]pyrene <br />ND <br />0.10 " <br />Benzyl alcohol <br />ND <br />0.10 " <br />Bis(2-chloroethoxy)methane <br />ND <br />0.20 " <br />Bis(2-chloroethyl)ether <br />ND <br />0.10 " <br />Bis(2-chloroisopropyl)ether <br />ND <br />0.10 " <br />Bis(2-ethythexyl)phthalate <br />ND <br />0.50 " <br />4-Bromophenyl phenyl ether <br />ND <br />0.20 " <br />Butyl benzyl phthalate <br />ND <br />0.50 " <br />4-Chloroaniline <br />ND <br />0.50 " <br />2-Chloronaphthalene <br />ND <br />0.10 " <br />4-Chloro-3-methylphenol <br />ND <br />0.10 " <br />2 -Chlorophenol <br />ND <br />0.10 " <br />4-Chlorophenyl phenyl ether <br />ND <br />0.20 " <br />Chrysene <br />ND <br />0.10 <br />Dibenz (a,h) anthracene <br />ND <br />0.10 " <br />Dibenzofuran <br />ND <br />0.10 " <br />Di -n -butyl phthalate <br />ND <br />0.50 " <br />1,2 -Dichlorobenzene <br />ND <br />0.10 " <br />1,3 -Dichlorobenzene <br />ND <br />0.10 " <br />1,4 -Dichlorobenzene <br />ND <br />0.20 " <br />3,3'-Dichlorobenzidine <br />ND <br />0.50 " <br />2,4-Dichlorophenol <br />ND <br />0.10 " <br />Diethyl phthalate <br />ND <br />0.50 " <br />2.4 -Dimethylphenol <br />ND <br />0.20 " <br />Dimethyl phthalate <br />ND <br />0.10 " <br />4,6-Dinitro-2-methvlphenol <br />ND <br />0.50 " <br />2.4-Dinitrophenol <br />ND <br />0.50 " <br />Sequoia Analytical - Sacramento <br />The results in this report apply to the samples analyzed to accordance with the churn or <br />custody document. This analytical report must be reproduced in its entirem <br />Page 15 of 20 <br />