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January 9, 2018 Lab ID : STK1755503 <br />Pactiv Packaging Inc. Customer : 3-17694 <br />Quality Control - Organic <br />Constituent <br />Method Date/11) Type I nits Colic. QC Data <br />DQO Note <br />Organic <br />ieth l hthalate <br />82700 12/28/17:219419SBL CCV m 80.00 113% <br />70-130 <br />imeth I hthalate <br />8270C 12/28/17:219419SBL CCV m 80.00 99.9% <br />70-130 <br />Di-n-butylphthalate 8270C 12/28/17:219419SBL CCV m 80.00 107% <br />70-130 <br />Di-n-octylphthalate 8270C 12128/17:219419SBL CCV m 80.00 99.6% <br />80-120 <br />luoranthene <br />8270C 12/28/17:219419SBL CCV m 80.00 114% <br />80-120 <br />luorene <br />8270C 12/28/17:219419SBL CCV m 80.00 97.7% <br />70-130 <br />exachlorobenzene 8270C 12/28/17:219419SBL CCV m 80.00 99.3% <br />70-130 <br />exachlorobutadiene 8270C 12/28/17:219419SBL CCV m 80.00 118% <br />80-120 <br />exachloroc clo entadiene 8270C 12/28/17:219419SBL CCV m 80.00 108% <br />70-130 <br />exachloroethane <br />8270C 12128/17:219419SBL CCV m 80.00 98.5% <br />70-130 <br />Indeno 1,2,3-c,d <br />ene 8270C 12/28/17:219419SBL CCV m 80.00 109% <br />70-130 <br />so horone <br />8270C 12/28/17:219419SBL CCV m 80.00 98.9% <br />70430 <br />Naphthalene <br />8270C 12/28/17:219419SBL CCV m 80.00 114% <br />70-130 <br />Nitrobenzene <br />8270C 12/28/17:219419SBL CCV m 80.00 96.0% <br />70-130 <br />Nitrobenzene -d5 <br />8270C 12/28/17:219419SBL CCV m 50.00 92.5% <br />70-130 <br />Nitrosodimethlamine 8270C 12/28/17:219419SBL CCV m 80.00 109% <br />70-130 <br />Nitrosodi-N- ro <br />lamine 8270C 12/28/17:219419SBL CCV m 80.00 92.1% <br />70-130 <br />Nitrosodi hen lamine 8270C 12/28/17:219419SBL CCV m 80.00 103% <br />80-120 <br />Chloro -m -cresol <br />8270C 12/28/17:219419SBL CCV m 80.00 102% <br />80-120 <br />Pentachlorophenol <br />8270C 12/28/17:219419SBL CCV m 80.00 114% <br />80-120 <br />Phenanthrene <br />8270C 12/28/17:219419SBL CCV in 80.00 111 % <br />70-130 <br />Phenol <br />8270C 12128/17:219419SBL CCV m 80.00 102% <br />80-120 <br />Phenol -d6 <br />8270C 12/28/17:219419SBL CCV m 100.0 106% <br />70-130 <br />-Te hen 1-d 14 <br />8270C 12/28/17:219419SBL CCV m 50.00 93.3% <br />70-130 <br />Pyrene <br />8270C 12/28/17:219419SBL CCV m 80.00 90.8% <br />70-130 <br />Pyridine <br />8270C 12/28/17:219419SBL CCV m 80.00 111 % <br />70-130 <br />Definition <br />CCV <br />Continuing Calibration Verification - Analyzed to verify the instrument calibration is within criteria. <br />Blank <br />: Method Blank - Prepared to verify that the preparation process is not contributing contamination to the samples. <br />LCS <br />: Laboratory Control Standard/Sample - Prepared to verify that the preparation process is not affecting analyte recovery. <br />: Matrix Spikes - A random sample is spiked with a known amount of analyte. The recoveries are an indication <br />of how that sample <br />MS <br />matrix affects analyte recovery. <br />: Matrix Spike Duplicate of MS/MSD pair - A random sample duplicate is spiked with a known amount of analyted. The recoveries <br />MSD <br />are an indication of how that sample matrix affects analyte recovery. <br />: Blank Spikes - A blank is spiked with a known amount of analyte. It is prepared to verify that the preparation <br />process is not <br />BS <br />affecting analyte recovery. <br />: Blank Spike Duplicate of BS/BSD pair - A blank duplicate is spiked with a known amount of analyte. It is prepared to verify that <br />BSD <br />the preparation process is not affecting analyte recovery. <br />: MS/MSD Relative Percent Difference (RPD) - The MS relative percent difference is an indication of precision for the preparation <br />MSRPD <br />and analysis. <br />: BS/BSD Relative Percent Difference (RPD) - The BS relative percent difference is an indication of precision <br />for the preparation <br />BSRPD <br />and analysis. <br />ND <br />: Non -detect - Result was below the DQO listed for the analyte. <br />D O <br />: Data Quality Objective - This is the criteria against which the quality control data is compared. <br />Explanation <br />360 <br />: CCV above Acceptance Range (AR). Samples which were non detect for this analyte were accepted. <br />435 <br />: Sample matrix may be affecting this analyte. Data was accepted based on the LCS or CCV recovery. <br />436 <br />Blank Spike (BS) not within Acceptance Range (AR). Data was accepted based on the LCS or CCV recovery. <br />Page 17 of 21 <br />