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California Environmental Protection Agency <br />For ECL No.: <br />AQ00950 <br />Department of Toxic Substances Control <br />to <br />AQ00959 <br />Environmental Chemistry Laboratory (Inorganic Section) <br />Authorization No.: <br />06ECO150 <br />700, Heinz Ave., Suite 100, Berkeley, CA 94710 <br />Page <br />2 <br />Phone: (510) 540-3003 <br />of <br />2 <br />ANALYTICAL LABORATORY REPORT - For Total <br />Metal Analysis <br />solid <br />Requestor's Name: Alex Baillie <br />Liquid, AqueouE <br />Limit <br />Address: 8800 Cal Center Drive <br />Date Collected: <br />1/18/2007 <br />Sacramento CA 95826 <br />Date Received: <br />1/18/2007 <br />Site of Sampling: Lodi Chrome <br />Date Digested: <br />1/23/2007 <br />316 North Main St <br />Date Analyzed: <br />1/25/2007 <br />Lodi CA 95240 <br />0.05 <br />_ <br />Barium -Ba <br />Analytical Samples are digested with 1:1 HNO3 (and 30% H2O2, and 1:1 HCI, <br />if applicable) over a hot plate. <br />Digests <br />Procedure: are cooled, filtered and made to final volume with deionized H2O. Metal analysis of the digests is by <br />EPA -SW 846 ICPAES (EPA #6010B). <br />0.04 <br />Beryllium -Be <br />Method: 30508 for snilds: 3010A for liquids: 3005A for drinkina water. <br />Units: ma/Ka <br />ND <br />ECL Number: <br />F A-QO0955 <br />A000956 <br />A000957 <br />A000958 <br />AQ00959 <br />Method <br />Method <br />Collector's No.: <br />RH6 <br />RH7 <br />RH8 <br />_ RH9 <br />Solid <br />RH10 _ <br />solid <br />__B_laan_k_____ <br />Detection <br />_ <br />Sample Type: <br />solid <br />Liquid, Aqueou <br />Liquid, AqueouE <br />Limit <br />Analyte <br />_ ND <br />291 <br />ND _ <br />Arsenic -As <br />ND <br />2.02 <br />ND <br />ND <br />0.05 <br />_ <br />Barium -Ba <br />_ <br />54.8 <br />NO <br />_ _ _ <br />ND <br />483 <br />ND <br />0.04 <br />Beryllium -Be <br />_ <br />ND <br />NO <br />ND <br />_ <br />ND <br />_ <br />ND <br />ND <br />0.01 <br />Cadmium -Cd <br />ND <br />ND <br />1.38 <br />29.0 <br />44.0 <br />NO <br />0.02 <br />Chromium -Cr <br />165 <br />117 <br />121000 <br />3520 <br />12500 <br />ND <br />0.04 <br />Cobalt -Co <br />51.2 <br />ND <br />17.2 <br />24.8 <br />24.7 <br />ND <br />0.03 <br />_ <br />Copper -Cu <br />8440 <br />22.6 <br />3410 <br />19700 <br />7280 <br />ND <br />0.1 <br />Lead -Pb <br />237 <br />116 <br />16.6 <br />2540 <br />8050 <br />ND <br />0.05 <br />Molybdenum -Mo <br />7.62 <br />5.95 <br />2.32 <br />3.86 <br />7.53 <br />ND <br />0.05 <br />Nickel -Ni <br />23800 <br />ND <br />1030 <br />3860 <br />9300 <br />ND <br />0.05 <br />Selenium -Se <br />ND <br />ND <br />ND <br />ND <br />ND <br />ND <br />0.05 <br />Thallium -TI <br />ND <br />NQ <br />_ <br />15.8 <br />ND <br />2.31 _ <br />ND <br />0.04 <br />Vanadium -V <br />32.0 <br />0.62 <br />ND <br />_ <br />ND <br />ND <br />ND <br />0.02 <br />0.04 <br />Zinc -Zn <br />7780 <br />3930 <br />_ <br />771 <br />1990 <br />3930 <br />ND <br />comments: ND=Not Detected <br />Staff Chemist Date <br />Merlyn De Guzman <br />Section Lead Chemist Date <br />1 Jarnail Garcha <br />Sample Prepared By <br />Dinesh Chand <br />,; 0-_� <br />Date <br />