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McCalIlabell Analytical, Inc. <br />"When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Web: www.mc=pbell.com E-mail: main@mccampbell.com <br />Telephone: 877-252-9262 Fax: 925-252-9269 <br />GeoRestoration, Inc. <br />585 Emory Street <br />San Jose, CA 95110 <br />Client Project ID: # 0837; Former Lodi <br />Chrome <br />Date Sampled: <br />10/09/08 <br />Date Received: 10/10/08 <br />Client Contact: Roger Dockter <br />Date Extracted: 10/10/08 <br />Client P.O.: <br />Date Analyzed 10/13/08 <br />Volatile Organics by P&T and GC/MS (Basic Target List) [Encore Sampling* <br />Extraction Method: SW5035 Analytical Method: SW8260B Work Order: 0810269 <br />Lab ID <br />0810269-OIOA <br />Client ID <br />SS -8d 1.0 <br />Matrix <br />Soil <br />Compound* <br />Concentration <br />DF <br />eportit <br />Rng <br />Compound <br />Concentration * <br />DF <br />Reporting <br />Limit <br />Acetone <br />ND<O 047 <br />1.0 <br />0.05 <br />tert-Am 1 methyl ether TAME <br />ND<0.0047 <br />1.0 <br />0.005 <br />Benzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Bromobenzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Bromochloromethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />Bromodichlorom thane <br />ND<0.0047 <br />1.0 <br />0.005 <br />Bromoform <br />ND<0.0047 <br />1.0 <br />0.005 <br />Bromomethane <br />D<0.0047 <br />1.0 <br />0.005 <br />2-Butan ne MEK) <br />ND<0 019 <br />1.0 <br />0.02 <br />t -But I alcohol TBA <br />ND<0.047 <br />1.0 <br />0.05 <br />n -Butyl benzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />see-Butvl benzene <br />ND<0 0047 <br />1.0 <br />0.005 <br />tert-But I benzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Carbon Disulfide <br />ND<0.0047 <br />1.0 <br />1 0.005 <br />Carbon Tetrachloride <br />ND<0.0047 <br />1.0 <br />0.005 <br />Chlorobenzene <br />ND<0 0047 <br />1.0 <br />0.005 <br />Chloroethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />Chloroform <br />ND<0.0047 <br />1.0 <br />0.005 <br />Chloromethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />2-Chlorotoluene <br />D<0 0047 <br />1.0 <br />0.005 <br />4 -Ch1 rotoluene <br />ND<0.0047 <br />1.0 <br />0-005 <br />Dibrom chloromethane <br />ND<0.0047 <br />1'0 <br />0.005 <br />1 2-Dibromo-3-chloro ro ane <br />ND<0.0037 <br />1.0 <br />0.004 <br />1 2-Dibromoethane EDB <br />ND<0.0037 <br />1.0 <br />0.004 <br />i rom methane <br />ND<0.0047 <br />1.0 <br />0.005 <br />1.2 -Dichlorobenzene <br />ND<0.0047 <br />1.0 <br />0005 <br />13 -Dichlorobenzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />14 -Dichlorobenzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Dichlorodifluoromethane <br />ND<0.0047 <br />LO <br />0.005 <br />1 1-Dichl roethane <br />ND<0 0047 <br />1.0 <br />0.005 <br />1 2-Dichloroethane H 2 -DCA <br />ND<0.0037 <br />L0 <br />0.004 <br />] 1-Dichl roethene <br />ND<0.0047 <br />1.0 <br />00051 <br />cis - I 2-Dichloroethene <br />ND<0 0047 <br />1.0 <br />0.005 <br />trans -1 2-Dichloroethene <br />ND<0.0047 <br />1.0 <br />0.005 <br />1 2 -Di hlor ro an <br />ND<0.0047 <br />1.0 <br />0.005 <br />1 3-Dichloro ro ane <br />ND<0.0047 <br />1.0 <br />0.005 <br />2 2-Dichloro ro ane <br />ND<0.0047 <br />1.0 <br />0.005 <br />1 1-Dichloro ro ene <br />ND<0.0047 <br />1.0 <br />0.005 <br />cis -I 3-Dichlor ro ene <br />ND<0.0047 <br />1.0 <br />0.005 <br />trans- 1 3 -Di hI r ro ene <br />ND<0 0 47 <br />1.0 <br />0.005 <br />Diiscir l ether DIPE <br />ND<0.0047 <br />1.0 <br />0.005 <br />Eth (benzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Ethyl er -but 1 eiller ETBE <br />ND<0.0047 <br />1.0 <br />0.005 <br />Freon 113 <br />N <0 093 <br />1.0 <br />0.1 <br />Hexachlorobutadiene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Hexachloroethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />2-Hexanone <br />ND<0.0047 <br />1.0 <br />0,005 <br />Iso ro (benzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />4 -Iso ro l toluene <br />ND<0 0047 <br />1.0 <br />0.005 <br />Meth I -t -but I ether MTBE <br />ND<0.0047 <br />1.0 <br />1 0.005 <br />Methylene chloride <br />ND<0.0047 <br />1.0 <br />0.005 <br />4 -Meth I-2- entanone MIBK <br />ND<0.0047 <br />1.0 <br />0.005 <br />Na hth lene <br />ND<0.0047 <br />1.0 <br />0.005 <br />n -Pro I benzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Stvrene <br />ND<0 0047 <br />1.0 <br />0.005 <br />1.1 .1.2 -Tetrachloroethane <br />ND<0.0047 <br />1.0 <br />0,005 <br />1 1,2.2 -Tetrachloroethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />Tetrachloroethene <br />ND<0.0047 <br />1.0 <br />0.005 <br />Toluene <br />ND<0.0047 <br />1.0 <br />0.005 <br />1 2 3-Trichlorobenzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />1.2 4-Trichlorobenzene <br />ND<0.0047 <br />I.0 <br />0.005 <br />1 1 1 -Trichloroethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />11.2 -Trichloroethane <br />ND<0.0047 <br />L0 <br />0,005 <br />Trichloroethene <br />ND<0 00 7 <br />1.0 <br />0.005 <br />Trichlorofluoromethane <br />ND<0.0047 <br />1.0 <br />0.005 <br />1 2 3-Trichloro ro ane <br />ND<0.0047 <br />1.0 <br />0.005 <br />1 2 4-Trimethvlbenzene <br />ND<0.0047 <br />1.0 <br />0.0051 <br />3 5-Trimethvlbenzene <br />ND<0.0047 <br />1.0 <br />0.005 <br />< <br />< <br />Surrogate Recoveries <br />%SS1: <br />83 <br />%SS2: <br />95 <br />0 <br />Comments: a9 <br />* water and vapor samples are reported in pg/L, soil/sludge/solid samples in mg/kg, product/oil/non-aqueous liquid samples and all TCLP & SPLP extracts <br />are reported in mg/L, wipe samples in pg/wipe. <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis. <br /># surrogate diluted out of range or coelutes with another peak; &) low surrogate due to matrix interference. <br />a9) reporting limit near, but not identical to, our standard reporting limit due to variable Encore sample weight <br />DHS ELAP Certification 1644 4-1- Angela Rydelius, Lab Manager <br />