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McCampbell Analytical, Inc. <br />:,• <br />"When Oualitv Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Web: www.mccampbell.com E-mail: main r�hr rtccampbell.com <br />Telephone: 877-252-9262 Fax: 925-252-9269 <br />GeoRestoration, Inc. <br />585 Emory Street <br />San Jose, CA 95110Client <br />Client Project ID: # 0837; Former Lodi Date Sampled: 10/09/08 <br />Chrome Date Received: 10/10/08 <br />Client Contact: Roger Dockter Date Extracted: 10/10/08 <br />P.O.: Date Analyzed 10/18/08 <br />Extraction Method: SW3550C <br />Semi -Volatile Organics by GC/NIS (Basic Target List)* <br />Analytical Method: SW8270C <br />Work Order: <br />0810269 <br />Lab ID <br />0810269-004B <br />Client ID <br />SS -6d 1.0 <br />Matrix <br />Soil <br />Compound <br />Concentration * DF <br />Reporting <br />Limit <br />Compound <br />Concentration * <br />DF <br />Reponing <br />Limn <br />Acenaphthene <br />1.0 <br />0.33 <br />Acenaphthylene <br />ND <br />1.0 <br />0.33 <br />Acetochlor <br />1.0 <br />0.33 <br />Anthracene <br />ND <br />1.0 <br />0.33 <br />Benzidine <br />1.0 <br />1.6 <br />Benzoic Acid <br />ND <br />1.0 <br />1.6 <br />Benzo(a)anthracene <br />1.0 <br />0.33 <br />Benzo b fluoranthene <br />ND <br />1.0 <br />0.33 <br />Benzo k fluoranthene <br />1.0 <br />0.33 <br />Benzo h i e lene <br />ND <br />1.0 <br />0.33 <br />Benzo(a)pyrene <br />MND <br />1.0 <br />0.33 <br />Benzyl Alcohol <br />ND <br />1.0 <br />1.6 <br />1,1 -Biphenyl <br />1.0 <br />0.33 <br />Bis 2-chloroethox Methane <br />ND <br />1.0 <br />0.33 <br />Bis 2-chloroeth 1 Ether <br />1.0 <br />0.33 <br />Bis 2-chloroiso ro 1 Ether <br />ND <br />1.0 <br />0.33 <br />Bis 2-eth Ihex 1 Phthalate1.0 <br />0.33 <br />4-Bromo hen I Phen I Ether <br />ND <br />1.0 <br />0.33 <br />But Ibenz I Phthalate <br />1.0 <br />0.33 <br />4-Chloroaniline <br />ND <br />1.0 <br />0.66 <br />4 -Chloro -3 -meth I henol <br />1.0 <br />0.33 <br />2-Chlorona hthalene <br />ND <br />1.0 <br />0.33 <br />2 -Chloro henol <br />1.0 <br />0.33 <br />4 -Chloro hen I Phenyl Ether <br />ND <br />1.0 <br />0.33 <br />Chrysene <br />ND <br />1.0 <br />0.33 <br />Dibenzo a h anthracene <br />ND <br />1.0 <br />0.33 <br />Dibenzofuran <br />ND <br />1.0 <br />0.33 <br />Di -n -but I Phthalate <br />ND <br />1.0 <br />0.33 <br />12 -Dichlorobenzene <br />ND <br />1.0 <br />0.33 <br />1,3 -Dichlorobenzene <br />ND <br />1.0 <br />0.33 <br />1,4 -Dichlorobenzene <br />ND <br />1.0 <br />0.33 <br />3 3-Dichlorobenzidine <br />ND <br />1.0 <br />0.66 <br />2 4-Dichloro henol <br />ND <br />1.0 <br />0.33 <br />Diethyl Phthalate <br />ND <br />1.0 <br />0.33 <br />2,4 -Dimethyl henol <br />ND <br />1.0 <br />0.33 <br />Dimethyl Phthalate <br />ND <br />1.0 <br />0.33 <br />4 6-Dinitro-2-meth I henol <br />ND <br />1.0 <br />1.6 <br />2 4-Dinitro henol <br />ND <br />1.0 <br />1.6 <br />2 4-Dinitrotoluene <br />ND <br />1.0 <br />0.33 <br />2 6-Dinitrotoluene <br />ND <br />1.0 <br />0.33 <br />Di-n-oct I Phthalate <br />ND <br />1.0 <br />0.33 <br />1 2 -Di hen 1h drazinc <br />ND <br />1.0 <br />0.33 <br />Fluoranthene <br />ND <br />Lo <br />0.33 <br />Fluor ne <br />ND <br />1.0 <br />0.33 <br />Hexachlorobenzene <br />ND <br />1.0 <br />033 <br />Hexachlorobutadiene <br />ND <br />1.0 <br />0.33 <br />Hexachlorocy clo pentadiene <br />ND <br />1.0 <br />1.6 <br />Hexachloroethane <br />ND <br />1.0 <br />0.33 <br />Indeno (1,2.3 -cd) i)vrene <br />ND <br />1.0 <br />0.33 <br />I o horone <br />ND <br />1.0 <br />0.33 <br />2 -Meth Ina hthalene <br />ND <br />1.0 <br />0.33 <br />2 -Meth I henol (o-Cresol)ND <br />1.0 <br />0.33 <br />3 &/or 4 -Meth 1 henol m -Cres <br />ND <br />1.0 <br />P. <br />0.33 <br />Naphthalene <br />ND <br />1.0 <br />0.33 <br />2-Nitroaniline <br />ND <br />1.0 <br />1.6 <br />3-Nitroaniline <br />ND <br />1.0 <br />1.6 <br />4 -Ni roaniline <br />ND <br />1 0 <br />16 <br />Nitrobenzene <br />ND <br />1.0 <br />0.33 <br />2 -Nitro hen I <br />ND <br />1.6 <br />4-Nitr henol <br />ND <br />1.0 <br />1.6 <br />N-Nitrosodi hen lamine <br />ND <br />1.0 <br />0.33 <br />N-Nitrosodi-n-t)rovylamine <br />ND <br />1.0 <br />0.33 <br />Pent chloro henol <br />ND <br />1.0 <br />1.6 <br />Phenanthrene <br />ND <br />1.0 <br />0.33 <br />Phenol <br />6.4 1.0 <br />0.33 <br />P Yrene <br />ND <br />1.0 <br />0.33 <br />1.2 4-Trichlorobenzene <br />ND <br />1.0 <br />0.33 <br />2.4.5 -Tr chlorohenol <br />ND <br />1.0 <br />0.33 <br />Surrogate Recoveries (%) <br />°/ S1. <br />81 <br />% 2: <br />91 <br />S3: <br />97 <br />0/.SS4: <br />83 <br />0 <br />%R96. <br />RO <br />Comments: <br />* water samples in pg/L, soil/sludge/solid samples in mg/kg, wipe samples in µg/wipe, product/oil/non-aqueous liquid samples and all TCLP & <br />SPLP extracts are reported in mg/L. <br />ND means not detected above the reporting limit; N/A means analyte not applicable to this analysis. <br />#) surrogate diluted out of range; &) low or no surrogate due to matrix interference. <br />a3) sample diluted due to high organic content <br />DHS ELAP Certification 1644 --f-- Angela Rydelius, Lab Manager <br />