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+t , <br /> unStar 25712 Commercentre Drive <br /> Laboratories, Inc. Lake Forest,California 92630 <br /> 949.297.5020 Phone <br /> IuuG Qt:AI I':Y ANALY IICAL SF:RVII F. Nxim NNIDF <br /> 949.297.5027 Fax <br /> WGR Project: NuStar Stockton Terminal <br /> 11021 Winners Circle Suite 101 Project Number: (none] Reported: <br /> Los Alamitos CA,90720 Project Manager: Gray Martz 03/17/21 08:12 <br /> PL-9 @ V! <br /> T210804-25(Soil) <br /> Reporting <br /> Analyte Result Limit Units Dilution Batch Prepared Analyzed Method Notes <br /> SunStar Laboratories,Inc. <br /> Extractable Petroleum Hydrocarbons by 8015B <br /> C6-C12(GRO) ND 10 mg/kg 1 1031046 03/10/21 03/13/21 EPA8015B <br /> C13-C28(DRO) ND 10 " <br /> C29-C40(MORO) ND 10 " <br /> Surrogate:p-Terphenyl 92.6% 65-135 " <br /> Metals by EPA 6010B <br /> Lead 5.2 3.0 mg/kg 1 1031043 03/10/21 03/13/21 EPA 6010b <br /> Volatile Oreanic Coruvounds bv FPA Method 8260B <br /> Bromobenzene ND 2.5 uglkg k 1 1031037 03/10/21 03/12/21 EPA 8260B <br /> Bromochloromethane ND 2.5 " <br /> Bromodichloromethane ND 2.5 " <br /> Bromoform ND 2.5 <br /> Bromomethane ND 2.5 " <br /> n-Butylbenzene ND 2.5 " <br /> sec-Butylbenzene ND 2.5 " <br /> tert-Butylbenzene ND 2.5 " <br /> Carbon tetrachloride ND 2.5 <br /> Chlorobenzene ND 2.5 " <br /> Chloroethane ND 2.5 f " <br /> Chloroform ND 2.5 " <br /> Chloromethane ND 2.5 " <br /> 2-Chlorotoluene ND 2.5 " <br /> 4-Chlorotoluene ND 2.5 " <br /> Dibromochloromethane ND 2.5 " <br /> 1,2-Dibromo-3-chloropropane ND 5.0 " <br /> 1,2-Dibromoethane(EDB) ND 2.5 " <br /> Dibromomethane ND 2.5 " <br /> 1,2-Dichlorobenzene ND 2.5 " <br /> 1,3-Dichlorobenzene ND 2.5 " <br /> 1,4-Dichlorobenzene ND 2.5 " <br /> Dichlorodifluoromethane ND 2.5 " <br /> Ll-Dichloroethane ND 2.5 " <br /> SunStar Laboratories,Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Mike Jaroudi,Project Manager I Page 82 of 105 <br />