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+1'..' <br /> nStar 25712 Commercentre Drive <br /> Laboratories, Inc. Lake Forest,California 92630 <br /> 949.297.5020 Phone <br /> IDING QUALM Y ANALN IICAL SFAvicts NA;1o'4win'r:. <br /> 949.297.5027 Fax <br /> WGR Project: NuStar Stockton Terminal <br /> 11021 Winners Circle Suite 101 Project Number: [none] Reported: <br /> Los Alamitos CA,90720 Project Manager: Gray Martz 03/17/21 08:12 <br /> Metals by EPA 6010B-Quality Control <br /> SunStar Laboratories,Inc. <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Univ Level Result %REC Limits RPD Limit Notes <br /> Batch 1031031-EPA 3050B <br /> Blank(1031031-BLKI) Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead ND 3.0 mg/kg <br /> LCS(1031031-BS1) Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead 90.8 3.0 mg/kg 100 90.8 75-125 <br /> Matrix Spike(1031031-MSI) Source:T210804-01 Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead 51.4 3.0 mg/kg 91.7 3.45 52.2 75-125 QM-05 <br /> Matrix Spike Dup(1031031-MSDI) Source:T210804-01 Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead 52.7 3.0 mg/kg 95.2 3.45 51.7 75-125 2.54 20 QM-05 <br /> Batch 1031043-EPA 3050B <br /> Blank(1031043-BLKI) Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead ND 3.0 mg/kg �Prepared: <br /> LCS(1031043-BS1) 03/10/21 Analyzed:03/13/21 <br /> Lead 97.9 3.0 mg/kg 100 97.9 75-125 <br /> I <br /> Matrix Spike(1031043-MSI) Source:T210804-21 Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead 75.7 3.0 mg/kg 100 2.54 73.1 75-125 QM-05 <br /> Matrix Spike Dup(1031043-MSD1) Source:T210804-21 Prepared:03/10/21 Analyzed:03/13/21 <br /> Lead 70.4 3.0 mg/kg 93.5 - 2.54 72.6 75-125 7.16 20 QM-05 <br /> SunStar Laboratories,Inc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Mike Jaroudi,Project Manager Page 89 0f 105 <br />