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—� Performance Analytical Inc. <br /> —� Air Quality Laboratory <br /> A Division of Columbia Analytical Services,Inc. <br /> An Employee Owned Company <br /> LABORATORY REPORT <br /> Client: IT CORPORATION Date of Report: 07/07/00 <br /> Address: 1433 N. Market Boulevard Date Received: 06/20/00 <br /> Sacramento, CA 95834-1943 PAI Project No: P2001500 <br /> Contact: Mr. Charles Metzinger Purchase Order: 147554 OP <br /> Client Project ID: San Joaquin County/Corral Hollow Landfill <br /> #809251/01030000 <br /> Three(3) Stainless Steel Summa Canisters labeled: "GW-1" "GW-2" "GW-3" <br /> The samples were received at the laboratory under chain of custody on June 20, 2000. The samples were <br /> received intact. The dates of analyses are indicated on the attached data sheets. <br /> Volatile Organic Compound Analysis <br /> The samples were analyzed by combined gas chromatography/mass spectrometry (GC/MS) for volatile <br /> organic compounds. The analyses were performed according to the methodology outlined in EPA <br /> Method TO-14A. The analyses were performed by gas chromatography/mass spectrometry, utilizing a <br /> direct cryogenic trapping technique. The analytical system used was comprised of a Hewlett Packard <br /> Model 5973 GC/MS/DS interfaced to a Tekmar AutoCan Elite whole air inlet system/cryogenic <br /> concentrator. A 100% Dimethylpolysiloxane capillary column (RT.-I, Restek Corporation, Bellefonte, <br /> PA)was used to achieve chromatographic separation. <br /> The results of analyses are given on the attached data sheets. <br /> Reviewed and Approved: TRed and Approved: <br /> �1It <br /> Wade Henton Chris Parnell <br /> Analytical Chemist Senior Chemist <br /> 2665 Park Center Drive,Suite D,Simi Valley.California 93065•Phone(805)526-7161•Fax(805)526-7270 <br />