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1534 Willow Pass Road,Pittsburg,CA 94565-1701 <br /> /-\,O McCampbell Analytical, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 <br /> "When ali(v Counts" http://www.mccampbell.com/E-mail:main@tnccampbell.com <br /> Pangea Environmental Svcs.,Inc. Client Project ID: #1540.001;Tracy Date Sampled: 07/08/13 <br /> Office Plaza <br /> Date Received: 07/09/13 <br /> 1710 Franklin Street,Ste.200 <br /> Client Contact: Tina De La Fuente Date Extracted: 07/12/13-07/15/13 <br /> Oakland,CA 94612 [Client P.O.: Date Analyzed: 07/12/13-07/15/13 <br /> Oxygenated Volatile Organics+ EDB and 1,2-DCA by P&T and CC/MS* <br /> Extraction Method: SW5030B Analytical Method:SW8260B Work Order. 1307227 <br /> Lah II) 1 3,07227-009C 1307227-027C <br /> Clicnt ID B-1 B-6 <br /> Reporting Limit for <br /> DF=1 <br /> Matrix W -- W <br /> DF 2.5 10 S <br /> Compound Concentration ug/kg µJI. <br /> tert-Amyl methyl ether(TAME) ND<1.2 ND<5.0 NA 0.5 <br /> t-Butyl alcohol(TBA) 43 ND<20 NA 2.0 <br /> 1,2-Dibromoethane(EDB) ND<1.2 ND<5.0 NA 0.5 <br /> 1,2-Dichloroethane(1,2-DCA) ND<1.2 N11<5.0 NA 0.5 <br /> Diisopropyl ether(D1PE) ND<1.2 ND<5.0 NA 0.5 <br /> Ethanol ND<120 ND<500 NA 50 <br /> Ethyl tert-butyl ether(ETBE) ND<1.2 ND<5.0 NA 0.5 <br /> Methanol ND<1200 ND<5000 NA 500 <br /> Methyl-t-butyl ether(MTBE) ND<1.2 ND<5.0 NA 0.5 <br /> Surrogate Recoveries(°/r) <br /> %SS1: 87 100 <br /> %SS2: 85 95 <br /> Comments c8,b6,bl a3 <br /> *water and vapor samples are reported inµg/L,soiVsludge/solid samples in mg/kg,product/oil/non-aqueous liquid samples and all TCLP&SPLP <br /> extracts are reported in mg/L,wipe samples inµg/wipe. <br /> ND means not detected above the reporting limit/method detection limit; N/A means analyte not applicable to this analysis; %SS=Percent Recovery of <br /> Surrogate Standard; DF=Dilution Factor <br /> #surrogate diluted out of range or coelutes with another peak,&)low surrogate due to matrix interference. <br /> a3)sample diluted due to high organic content. <br /> b 1)aqueous sample that contains greater than—1 vol.%sediment <br /> b6)lighter than water immiscible sheen/product is present <br /> c8 sample pH is greater than 2 <br /> CDPH ELAP 1644 NELAP 12283CA KF Analyst's Initiall Angela Rydelius,Lab Manager <br /> Page 7 of 14 <br />