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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 Fax 717-656-2681•www.lancasterlabs.com <br /> Pagel of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgmt Co Group Number: 1203974 <br /> Reported: 08/13/10 at 02:10 PM <br /> Matrix QC may not be reported if site-specific QC samples were not <br /> submitted. In these situations, to demonstrate precision and accuracy at <br /> a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br /> method. <br /> Laboratory Compliance Quality Control <br /> BlankBlank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL** Loo Units %REC %REC Limits RPD RPD Max <br /> Batch number: A102031AA Sample number(s) : 6037223-6037225 <br /> Benzene N.D. 0.0005 0.005 mg/kg 113 80-120 <br /> Ethylbenzene N.D. 0.001 0.005 mg/kg 111 80-120 <br /> Toluene N.D. 0.001 0.005 mg/kg 111 80-120 <br /> Xylene (Total) N.D. 0.001 0.005 mg/kg 104 80-120 <br /> Batch number: 10202SLB026 Sample number(s) : 6037223-6037225 <br /> Acenaphthene N.D. 0.00067 0.0017 mg/kg 86 87 73-104 1 30 <br /> Acenaphthylene N.D. 0.00033 0.0017 mg/kg 86 86 67-100 1 30 <br /> Anthracene N.D. 0.00033 0.0017 mg/kg 89 89 69-107 0 30 <br /> Benzo(a)anthracene N.D. 0.00067 0.0017 mg/kg 89 90 74-112 1 30 <br /> Benzo(a)pyrene N.D. 0.00067 0.0017 mg/kg 89 89 70-109 0 30 <br /> Benzo(b)fluoranthene N.D. 0.00067 0.0017 mg/kg 86 86 73-123 0 30 <br /> Benzo(g,h,i)perylene N.D. 0.00067 0.0017 mg/kg 77 80 62-128 3 30 <br /> Benzo(k)fluoranthene N.D. 0.00067 0.0017 mg/kg 96 94 65-130 1 30 <br /> Chrysene N.D. 0.00033 0.0017 mg/kg 91 93 79-111 2 30 <br /> Dibenz(a,h)anthracene N.D. 0.00067 0.0017 mg/kg 79 81 69-128 3 30 <br /> Fluoranthene N.D. 0.00067 0.0017 mg/kg 89 90 78-114 1 30 <br /> Fluorene N.D. 0.00067 0.0017 mg/kg 88 89 75-110 1 30 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.00067 0.0017 mg/kg 80 82 71-127 2 30 <br /> 1-Methylnaphthalene N.D. 0.00067 0.0017 mg/kg 96 95 72-114 1 30 <br /> 2-Methylnaphthalene N.D. 0.00067 0.0017 mg/kg 80 80 62-115 0 30 <br /> Naphthalene N.D. 0.00067 0.0017 mg/kg 89 89 67-105 0 30 <br /> Phenanthrene N.D. 0.00067 0.0017 mg/kg 90 90 76-109 0 30 <br /> Pyrene N.D. 0.00067 0.0017 mg/kg 97 91 71-109 6 30 <br /> Batch number: 102020027A Sample number(s) : 6037223-6037225 <br /> C10-C36 N.D. 4.0 12 mg/kg <br /> Total TPH N.D. 4.0 12 mg/kg 90 72-125 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> Ms MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name RE %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: A102031AA Sample number(s) : 6037223-6037225 UNSPK: P035036 <br /> Benzene 120 121 55-143 2 30 <br /> Ethylbenzene 122 122 44-141 2 30 <br /> Toluene 122 123 50-146 2 30 <br /> Xylene (Total) 112 113 44-136 2 30 <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />