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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 Fax:717-656-2681•www.lancasterlabs.com <br /> Page 1 of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgmt Co Group Number: 1204353 <br /> Reported: 08/18/10 at 01:15 PM <br /> Matrix QC may not be reported if site-specific QC samples were not <br /> submitted. In these situations, to demonstrate precision and accuracy at <br /> a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br /> method. <br /> Laboratory Compliance Quality Control <br /> Blank Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL** Loo Units %REC %REC Limits RPD RPD Max <br /> Batch number: B102051AA Sample number(s) : 6039944-6039949 <br /> Benzene N.D. 0.0005 0.005 mg/kg 104 101 80-120 3 30 <br /> Ethylbenzene N.D. 0.001 0.005 mg/kg 98 94 80-120 5 30 <br /> Toluene N.D. 0.001 0.005 mg/kg 101 96 80-120 4 30 <br /> Xylene (Total) N.D. 0.001 0.005 mg/kg 98 95 80-120 3 30 <br /> Batch number: 10209SLB026 Sample number(s) : 6039944-6039949 <br /> Acenaphthene N.D. 0.00067 0.0017 mg/kg 94 73-104 <br /> Acenaphthylene N.D. 0.00033 0.0017 mg/kg 96 67-100 <br /> Anthracene N.D. 0.00033 0.0017 mg/kg 96 69-107 <br /> Benzo(a)anthracene N.D. 0.00067 0.0017 mg/kg 98 74-112 <br /> Benzo(a)pyrene N.D. 0.00067 0.0017 mg/kg 96 70-109 <br /> Benzo(b)fluoranthene N.D. 0.00067 0.0017 mg/kg 93 73-123 <br /> Benzo(g,h,i)perylene N.D. 0.00067 0.0017 mg/kg 98 62-128 <br /> Benzo(k)fluoranthene N.D. 0.00067 0.0017 mg/kg 94 65-130 <br /> Chrysene N.D. 0.00033 0.0017 mg/kg 99 79-111 <br /> Dibenz(a,h)anthracene N.D. 0.00067 0.0017 mg/kg 97 69-128 <br /> Fluoranthene N.D. 0.00067 0.0017 mg/kg 97 78-114 <br /> Fluorene N.D. 0.00067 0.0017 mg/kg 98 75-110 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.00067 0.0017 mg/kg 99 71-127 <br /> 1-Methylnaphthalene N.D. 0.00067 0.0017 mg/kg 103 72-114 <br /> 2-Methylnaphthalene N.D. 0.00067 0.0017 mg/kg 87 62-115 <br /> Naphthalene N.D. 0.00067 0.0017 mg/kg 95 67-105 <br /> Phenanthrene N.D. 0.00067 0.0017 mg/kg 98 76-109 <br /> Pyrene N.D. 0.00067 0.0017 mg/kg 98 71-109 <br /> Batch number: 102080024A Sample number(s) : 6039944-6039949 <br /> C10-C36 N.D. 4.0 12 mg/kg <br /> Total TPH N.D. 4.0 12 mg/kg 112 72-125 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: B102051AA Sample number(s) : 6039944-6039949 UNSPK: P036712 <br /> Benzene 110 55-143 <br /> Ethylbenzene 136 44-141 <br /> Toluene 142 50-146 <br /> Xylene (Total) 237* 44-136 <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />