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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 Fax:717-656-2681•www.lancasterlabs.com <br /> Page l of 2 <br /> Sample Description: SB-47-W-100721 Grab Water LLI Sample # WW 6039952 <br /> US Can - Welty Road SAIC LLI Group # 1204354 <br /> 35275 Welty Rd-Vernalis SLO607746470 SB-47 Account # 11413 <br /> Project Name: US Can-Welty Road <br /> Collected: 07/21/2010 16:30 by SS Chevron Environmental Mgmt Co <br /> 6111 Bollinger Canyon Road <br /> Submitted: 07/23/2010 10:10 BR1Y/3484 <br /> Reported: 09/03/2010 10:15 San Ramon CA 94583 <br /> Discard: 10/04/2010 <br /> VER47 SDG#: OVX42-03 <br /> As Received <br /> CAT As Received Dilution <br /> No. Analysis Name CAS Number Program <br /> Result RL Factor <br /> GC/MS Volatiles SW-846 8260B 25mL ug/1 ug/l <br /> purge <br /> 02898 Benzene 71-43-2 N.D. 0.1 1 <br /> 02898 Ethylbenzene 100-41-4 N.D. 1.0 1 <br /> 02898 Toluene 108-88-3 N.D. 1.0 1 <br /> 02898 Xylene (Total) 1330-20-7 N.D. 1.0 1 <br /> GC/MS Semivolatiles SW-846 8270C LVI ug/l ug/l <br /> 06570 Acenaphthene 83-32-9 0.27 0.010 1 <br /> 06570 Acenaphthylene 208-96-8 0.020 0.010 1 <br /> 06570 Anthracene 120-12-7 0.010 0.010 1 <br /> 06570 Benzo(a)anthracene 56-55-3 0.024 0.010 1 <br /> 06570 Benzo(a)pyrene 50-32-8 0.021 0.0030 1 <br /> 06570 Benzo(b)fluoranthene 205-99-2 0.022 0.010 1 <br /> 06570 Benzo(g,h,i)perylene 191-24-2 0.018 0.010 1 <br /> 06570 Benzo(k)fluoranthene 207-08-9 N.D. 0.010 1 <br /> 06570 Chrysene 218-01-9 0.033 0.010 1 <br /> 06570 Dibenz(a,h)anthracene 53-70-3 0.0068 0.0030 1 <br /> 06570 Fluoranthene 206-44-0 0.080 0.010 1 <br /> 06570 Fluorene 86-73-7 0.081 0.010 1 <br /> 06570 Indeno(1,2,3-cd)pyrene 193-39-5 0.013 0.010 1 <br /> 06570 1-Methylnaphthalene 90-12-0 0.058 0.0039 1 <br /> 06570 2-Methylnaphthalene 91-57-6 0.035 0.0039 1 <br /> 06570 Naphthalene 91-20-3 0.13 0.050 1 <br /> 06570 Phenanthrene 85-01-8 0.14 0.010 1 <br /> 06570 Pyrene 129-00-0 0.12 0.010 1 <br /> The recoveries of several compounds were outside of QC limits in the LCS/LCSD. <br /> No further action was taken. <br /> GC Extractable TPH SW-846 8015B ug/1 ug/1 <br /> 06912 TPH-DRO water C10-C25 n.a. 100 50 1 <br /> The observed sample pattern is not typical of #2 fuel/diesel. It elutes in the <br /> DRO range later than #2 fuel and contains individual peaks eluting in the DRO <br /> range. <br /> GC Extractable TPH SW-846 8015B ug/l ug/l <br /> w/Si Gel <br /> 06913 TPH-DRO water C10-C25 w/Si Gel n.a. N.D. 50 1 <br /> General Sample Comments <br /> State of California Lab Certification No. 2501 <br /> All QC is compliant unless otherwise noted. Please refer to the Quality <br /> Control Summary for overall QC performance data and associated samples. <br /> #=Laboratory MethodDetection Linlit exceeded target detection linlit <br /> N.D.=Not detected at or above the Reporting Limit <br />