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01eurofins <br /> Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425•717-656-2300 Fax:717-656-2681•www.lancasterlabs.com <br /> Sample Description: SB-7-W-121213 Grab Water LLI Sample # WW 6896682 <br /> Highway 33 (Ahern Road) SAIC LLI Group # 1356656 <br /> Ahern Road - Vernalis T10000002723 SB-7 Account # 11413 <br /> Project Name: Ahern Road - Vernalis <br /> Collected: 12/13/2012 10:55 by SG Chevron Environmental Mgmt Cc <br /> 6101 Bollinger Canyon Road <br /> Submitted: 12/15/2012 09:05 Room 5384 <br /> Reported: 01/04/2013 12:58 San Ramon CA 94583 <br /> D13S7 <br /> As Received As Received <br /> CAT As Received Limit of Method Dilution <br /> No. Analysis Name CAS Number Result Quantitation* Detection Limit Factor <br /> GC/MS Volatiles SW-846 8260B 25mL ug/1 ug/l ug/1 <br /> purge <br /> 02898 Benzene 71-43-2 N.D. 0.5 0.1 1 <br /> 02898 Ethylbenzene 100-41-4 N.D. 0.5 0.1 1 <br /> 02898 Toluene 108-88-3 N.D. 0.5 0.1 1 <br /> 02898 Xylene (Total) 1330-20-7 N.D. 0.5 0.1 1 <br /> GC/MS Semivolatiles SW-846 8270C LVI ug/1 ug/1 ug/l <br /> 06570 Acenaphthene 83-32-9 0.019 0.0089 0.0030 1 <br /> 06570 Acenaphthylene 208-96-8 N.D. 0.0049 0.0020 1 <br /> 06570 Anthracene 120-12-7 0.0034 J 0.0059 0.0030 1 <br /> 06570 Benzo(a)anthracene 56-55-3 N.D. 0.0089 0.0030 1 <br /> 06570 Benzo(a)pyrene 50-32-8 N.D. 0.0089 0.0030 1 <br /> 06570 Benzo(b)fluoranthene 205-99-2 N.D. 0.0089 0.0030 1 <br /> 06570 Benzo(g,h,i)perylene 191-24-2 N.D. 0.012 0.0039 1 <br /> 06570 Benzo(k)fluoranthene 207-08-9 N.D. 0.0089 0.0030 1 <br /> 06570 Chrysene 218-01-9 N.D. 0.0049 0.0020 1 <br /> 06570 Dibenz(a,h)anthracene 53-70-3 N.D. 0.0089 0.0030 1 <br /> 06570 Fluoranthene 206-44-0 0.014 0.0059 0.0030 1 <br /> 06570 Fluorene 86-73-7 0.021 0.0059 0.0030 1 <br /> 06570 Indeno(1,2,3-cd)pyrene 193-39-5 N.D. 0.012 0.0039 1 <br /> 06570 1-Methylnaphthalene 90-12-0 0.0093 J 0.012 0.0039 1 <br /> 06570 2-Methylnaphthalene 91-57-6 0.0095 J 0.012 0.0039 1 <br /> 06570 Naphthalene 91-20-3 0.028 0.0089 0.0030 1 <br /> 06570 Phenanthrene 85-01-8 0.064 0.0089 0.0030 1 <br /> 06570 Pyrene 129-00-0 0.0083 J 0.0089 0.0030 1 <br /> The recovery for a target analyte(s) in the Laboratory Control <br /> Spike(s) is outside the QC acceptance limits as noted on the QC <br /> Summary. The following corrective action was taken: <br /> The sample was re-extracted outside the method required holding <br /> time and the QC is compliant. All results are reported from the <br /> first trial. Naphthalene was the only target compound detected in the both <br /> extractions of the sample. The following compounds were detected in the re- <br /> analysis of the sample: <br /> benzo(b)fluoranthene <br /> benzo(k)fluoranthene <br /> indeno(1,2,3-cd)pyrene <br /> dibenz(a,h)anthracene <br /> benzo(g,h,i)perylene <br /> GC Petroleum SW-846 8015B ug/1 ug/l ug/1 <br /> Hydrocarbons <br /> 06912 TPH-DRO water C10-C25 n.a. N.D. 100 50 1 <br /> *=This limit was used in the evaluation of the final result <br /> Page 4 of 13 <br />