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FREEDMAN & BRUYA, INC. <br /> EWRCNMEENTAL CHEMISTS <br /> Analysis For PNA Compounds By EPA Method 8270C SEM <br /> Client Sample ID: S13-9-45.0 Client: Geomatrix Consultants, Inc. <br /> Date Received: 05/24/02 Project: 5011.001 (Roberts Property) <br /> Date Extracted: 06/03/02 Lab ID: 205192-15 1110 <br /> Date Analyzed: 06/07/02 Data File: 060713.1) <br /> Matrix: Soil Instrument: GCMS3 <br /> Units: ug/kg(ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: %Recovery Limit Limit <br /> Anthracene-d10 86 43 109 <br /> Benzo(a)anthracene-d12 158 vo 65 134 <br /> Concentration: <br /> Compounds: ug/kg(ppb) <br /> Naphthalene <50 <br /> Acenaphthylene <50 <br /> Acenaphthene 240 <br /> Fluorene 450 <br /> Phenanthrene 880 <br /> Anthracene <50 <br /> Fluoranthene <50 <br /> Pyrene 100 <br /> Benz(a)anthracene 55 <br /> Chrysene 140 <br /> Benzo(b)fluoranthene <50 <br /> Benzo(k)fluoranthene <50 <br /> Benzo(a)pyrene <50 <br /> Indeno(1,2,3-ed)pyrene <50 <br /> Dibenzo(a,h)anthracene <50 <br /> Benzo(g,h,i)perylene X50 <br /> Note: The sample was diluted due to high levels of interfering compounds. Detection limits are raised <br /> due to dilution and surrogate recoveries may not be meaningful. <br /> vo - The value reported fell outside the control limits established for this analyte. <br /> 23 <br />