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FRIDMAN&BRUYA,INC. - - FRI DMAN&BRUYA,INC. <br /> ENVDtONA¢N'EALCHEMLBTS <br /> y BNYHtpNMENTALCHFMIBis <br /> I Analysis For PNA Compounds By EPAMethod8270C SIM - Analysis For PNA Compounds By EPA Method8270C SAE <br /> Clieot&nepl.m. S&165.0 Client Ommurne Conenatnta.Ino Client Sample D7: Method Week Client C .ria Core borne,Int <br /> -.l` Date Roecvca p I'm Pmjece 5011,001,1'"li8099 <br /> Dale R¢ceivea No[App5ceb4 Pmjst 601LOW.Fd 13WN3 <br /> Dao hlnNed: 08IIS89 Labor: 306093-6 Dao Emackd: MINI <br /> Dem Avalyzed 082283 Data Fie: 08=IZ Date Aanlyzca 06'l6'03 Lalowflail F: OBV7mb <br /> Mnkiz: Soil Imnummt OCM53 Metric Soli Dalorte He: CCM8.9 <br /> IMD <br /> }" Una. g&g Opb) OPmamn YA Unite: ughg(pPb) OPe+ator. YA <br /> 1 Ye <br /> -..-I Sunogaus: %Reaxery Limit upper <br /> Lower UPpee <br /> j Mtloee,A dl0 67 44 113 Sutropw: %Recover, Limo Limit <br /> T� Renm(e)nntIrneooedl2 70 fi5 134 Mthracme-10 84 M 113 <br /> Reora(pmWracened12 & 65 134 <br /> Caneenrntim: - <br /> Cmnpounde Concenneeoo: <br /> f' J ngag(pb) Compounds: ug/k"pb) <br /> Naphlbelene b Naphthalene b <br /> Arenapbthylene b Attnaphlete <$ <br /> AcmaPhthme b Acenaphthene .e5 <br /> Fluorene Finance. <br /> Ph.nanthrene b Ph anp ene b <br /> Mthracene b Mthn <br /> (- 3 Fluormthme e5 AA,hr ct.c4 <br /> .. Fluorenthene <br /> nz .r RenzWenti xme b 11 90—thzacene b <br /> (haeme <5 <br /> Rmm(b)Dumenthene <5 BeanoNluorenWme e5 <br /> Rmm(IORuamnthme c5 Bmm(gDuormthme b <br /> BIndm(R.3-4pyrene <6 Renio(e)p3'rane b <br /> Dlbmm(a,h)mWracene e5 Indeno(12.3�Pyrene b <br /> Nnze(gy,OPer,lene b Dibenzn(e,hAnthracme b <br /> &nzo(g.h,8peryleoe b <br /> V:d <br /> J.. <br /> i <br /> L : <br /> L� <br /> 16 <br /> 17 <br /> FR®MAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> i- ENYIRONMEN'FALC�Mi51'S F3iVHtONb1ENTAL CUEh4S'FS <br /> J1 Datedltnport:08126103 Da eoERepord 0626103 <br /> Date Received OB/1&03 Date Received,08/IW3 <br /> Project, 5011.002,F&HI308093 Project: 5011.002,F&HI308093 <br /> QUALITYASSURANCE RESULTS FROM THE ANALYSIS OF SOIL SAMPLES QUALITYASSURANCE RESULTS FORTHE ANALYSIS OF SOIL SAMPLES <br /> FOR TOTAL PETROLEUM HYDROCARBONS AS CRUDE OD, <br /> USING EPA METHOD 8015M FOR VOLATILES BY EPA METHOD 8260E <br /> - <br /> E.3 Istommr,Code:8o8o99A1(Ouplice4 <br /> LahomtoryCode:3o8oC4-O6(DupDtnm) <br /> Relative percencs Ablative Perms[ <br /> Repomiog Sample DuPSmm Diierenee Reporting Sample DItci®le DinAltm <br /> a.p Malvre Dmfs Aeaulr Aoeul If-i 2N - Ile g(pp Rnulr Result (I.imi[201 <br /> Ltude Ol yg/6(Ppm/ V`0 <Sll rtm !moon. Pglg OP.) <10m <D.CRS <br /> y3 <br /> Ethyl... <br /> Vg/6 OP.) ACUS mWs one <br /> Ethylene A919NPm1 A.(U8 A.005 A. <br /> tabommry Code:3LU0W-I pMntix 6pLLe) m.Xylene A919OP-) <0,00 <0005 Ann <br /> Pereent Pereen[ o-Wene Pglg pp.) A005 AA3$ nm <br /> Repormg Spike SwPk Reon,er, 8ecmery AcceAmrmA RPD <br /> �S Amlv(e Unna Level Result MS MBD Cri (Li yAR <br /> .g_. Crude Od vvg pp.) IN 550 1� 109 65.135 I Laborauo' o :908044.069dntriz SPOte) <br /> T Pemmt Percent <br /> Repncting Spike SwPle Rwae, Ramvery Acceptance RPD <br /> l.ehmamry Cade:fahonmry Carmol Semple Male Unid Level Resu[ MS MSD (ki (Lim' 001 <br /> Pemnt Percent Benzene K/g Npm) am Rams 118 111 76130 6 <br /> - <br /> P.—. !Pike Rawer, mA <br /> Reaer, Pt•^... RPD Toluene RIg(ppmA. <br /> ) am 005 114 IV 70-130 6 <br /> Analvle U)m Lw) IGB LG80 Cri " 0-m' P(0 - Elhllbeomne P6,,(pp.) am A.005 118 112 70.130 6 <br /> Ccude Od Age:OP.) 500 110 103 M-I35 t mXYlene pglg(ppm) am A005 IPO— 112 70.130 7 <br /> o.Xylene AgIff Opm) am <9.005 IIR 110 7x130 7 <br /> m.Tle m)yle wv nadetecmdmmoor more o[lhe dup5mmamlysm Therefore,mkvlatioo aE lolenotery Code:Isbomtor,Caonal!ample <br /> f _ the RPDuootapPGcable. Pent Percent <br /> I Reporting Spike R or, anoveeY jtcceplenca RPD <br /> ~t _: Malvfe Un'n 4051 101 -CSD 7" (1 0 2 <br /> LI Rmzene peg Opm) am 101 101 70.130 0 <br /> Tod umc W,(Ppeol am 97 86 7�130MIN 1Etloy - <br /> zo-Xlleo, nIg Npm) am IN 100 70.130 0 <br /> m�Xylme pglg Nps) 0.05 102 ID3 70-130 I <br /> ' a o-Xykne xg/g Op.) 0.05 102 102 70.130 0 <br /> 5 <br /> 1. m-The analyte was not denebclin meormore o[the dup4 cc An9ysa.lbesefore,ealculatim of <br /> Ne RPDu not applicable. <br /> Y: f <br /> ;a'v`: 18 19 <br />