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FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> ENVBtONAtENN'fAL CNEhBST3 ENVIRONMENTAL CHEFIISTS <br /> Date of Repo=08AXV03 DateofRepo=08/26/03 <br /> Date Received 081/2/03 Date Received 08112108 <br /> Project: 5011.002,F&M 308108 Pgoj.t: 5011.002,F&BI 308108 t <br /> QUALITY ASSURANCE RESULTS FROM THE ANALYSIS OFSOIL SAMPLES QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF SOIL SAMPLES <br /> FOR TOTAL PETROLEUM HYDROCARBONSAS CRUDE OIL FOR VOLATILES BY EPA METHOD 82606 <br /> USING EPA METHOD 8015M <br /> IabmanryCode:SO6pC401(DapBraW Iah uCode:303NIN(DupFvaw) AeLtiva Pmemt <br /> Eda4ePPa—nt <br /> Aepax6vg Sample DuDlkab Dille Reporting Semple DupBmn Di&raam <br /> Mslvn Unin Reaul[ R—Jl Udm'20) mgUnin Resin[ Rezul[ (Limit 20) <br /> Cxude OR wg(pp.) `fi0 `50 am llenxene Pat(ppa) 4.W5 M005 _ <br /> Toluene po"p-) 4.W5 4m <br /> Ex ylhenreae pg/g(pp.) RW5 '0.006 <br /> 1aWretary Code:908044-01 pGniz SNAeI m.XYleve nIg(pp.) A005 A005 <br /> Pertevt Pemmt aXyl.ne Peg(pp.) .4.W5 4.W5 <br /> RaPaNaH iP- Sampb Rawery Rcwery Ao-ePxaaea I1PD <br /> Mahn Uvin Level Result MS MSD Cri O-i 01 Lhoratosy Cade:lKXCX4W 0daniz SPiWJ <br /> Baa <br /> OR Pyh OpW sW 4o IW tW 651ss I P..t Pamen[ f,- <br /> Reporting SpAe Semple Remrary lt—r Amepxmm RPD <br /> I,pw.,Cade:LaMnbryConmpl Semple Mage Unita Iavel Rnult US MSD C.;,..:e (LiaRm <br /> Pemmt Pe—t Benzene ygg Npm) 0.05 `O.WS in Ill 7RIao 6 <br /> R Parsing Spike M ery Hemxery A ptavr0 -RPD Toluene n/g(ppm) 0.05 m.Ws 114 107 70.130 6 <br /> Malvte Unite Level I,CS ICSD Cris, ff.' .2T Eayb mmne nlg ppm) &W W005 113 112 70.130 6 <br /> Czude Od wu Npm) 600 IlR IN 65135 1 m-%Ylene wig(pp.) 0.05 4.W5 120 112 70.130 7 <br /> uXylme Pg/g Op.) am 4.005 Ila 110 76190 7 r' <br /> rw-The evalYn wss na[da[mndin one armmaofthe dup0un melyam.Therefore,ralmlatiep0( Lbarebry Cede:labanbry Canaml Samle <br /> p _ <br /> We RPD b..p, W. Partin[ Pero', <br /> Repmtiag spa. Ramey R—.1 Asmxmu RPD <br /> Melvn Unin Level IGS LCSD CnUm 05mit 20) .. <br /> Benzene pg/g.0pm) am 101 101 70130 0 <br /> Toluene wIg(ppm) 0.05 97 N 70130 1 <br /> ENYlbmune pg/g(.Pm) am IN IN 10130 0 <br /> m&ybna W19(mm) 0.W IN IN 76190 1 <br /> uXYlme "Ig(ppm) am 102 102 76120 0 <br /> We."RPD elsno[detecledin ovaamore oFdxe dupl'man analyses 7heretme,mlcWelianM <br /> _ is umRaDPbable. <br /> 20 21 <br /> FRIEDMAN&BRUYA,INC. —FRIEDMAN&BRUYA,INC. <br /> ENVIRONMENTAL CHEMISTS ENVIRONMENEALCH STS <br /> DateofRepo=08/26103 Dateof Repo= 08/26/03 <br /> Date Received 08/12103 <br /> Project 5011.002,F&BI 308108 Date Received 08/12/03 <br /> Project: 5011.002,F&B1308108 <br /> QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF SOIL SAMPLES QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF SOIL <br /> FOR VOLATILES BY EPA METHOD 82608 SAMPLES FOR PNA'S BY EPA METHOD 8270C SIM <br /> Gtumwu Code:308120.01 Mupli-w LeWrebry Code:308109W(DuPSvaW Rau..Peron[ ... <br /> Rdaive Pexwn[ Repvr6aH Semple Duplvan IBReren<e <br /> _ Reparcng S ,k D.,Uate DiEe:evee J U Result ReaWt (Limit 20) _ <br /> Melme Unin Resin[ Result (Limit 20) NaPM1Bmlene R&6 Npb) 4 <br /> Benzene pg/g op.) 4.05 4.05 Menapht ylene "&a NDN 4 4nm <br /> Toluene K1907m) 4.05 4.05 " xmapfithena V6Ag(ppb) 4 4nm <br /> EB.YBwnune pG/g Npm) 4.05 4.W Fluorine pg/k6(.Pb) `5 <br /> mp.XYlene MIC(ppm) `0.05 4.W `• <br /> a.Xylene pg/g pp.) 005 4.05 vin Pnffira neve Rag Npb) `5 4 <br /> Mxhnune Kg ppb) <br /> F7uouvtfieve MAC Npb) 4 4 <br /> ]aboremry Cade:Lehomnry Canxml Semple Pyrene P6Ag ppb) <br /> ) 4 4 _ <br /> Pe l Partes[ emx(a)anbreame Anftft(ppb) 4 4 <br /> Reporting I—el Recovery RICSIJ Acn rare RPD lkn s by Aft 0Pb) `5 `5 <br /> Benzes Unin [eel 198 97 77.112 (I.imi[20) BenraN)0uveanNme pg&g(ppb) `5 4 <br /> Benzene wg NPm1 25 93' 97 77IN 1 Benzo(k)pumethme p Ag(ppb) 4 `5 <br /> 7bluene p9hC(pp.) 25 97 W 77 IN 0 Benm(a1,2.3ne pgAg(ppb) 5 6 <br /> .-Xlbenune p6/6 Na) 25 10 95 70.130 0 ladero(1.blanpymne Pghg(Ppb) `5 4 <br /> m-Xylene pg/g Npm) 25 102 IN 70.190 2 OiSmza(a.M1)mrhrame Pf)kg Oph) `5 4 <br /> o-Xylme pg/g(pp-) 25 102 101 70130 1 BenrNg.h,OparYleae pgAB(pPb) <br /> Labmabry Cade:MINIM oust Spike) <br /> xw-7Lesnalynwazm[detcedn oveamore of Ne dup6mn manses Therefore,oalcun9vn o[ Pertmt Pertea[ <br /> Ne F1PD bna[aP09rabls Rmni. S d Sample Ram+ery R.awery Aaepxmm RPD <br /> al U' Leval 1 MS MSD Crinria O:mia W <br /> NepM1ahelene <br /> nA,(ppb) t70 4 82 65 6-117 9 <br /> AcenephNYlme pg&g(ppb) ❑0 4 92 59-115 5 <br /> AcmaphRrene p, (ppb) 170 4 a 33 92 59-114 5 <br /> Plum.¢ p,tAg(ppb) 170 4 01 89 61.113 6 <br /> Pheumbrme wkg(ppb) 170 e5 93 W 50122 9 <br /> mffi.me VVU(111) 170 4 78 83 50116 6 <br /> Fluvrenthma p,I,Nb) 170 `5 82 99 52124 8 <br /> Pyrtne p,AC Nb) 170 GS 94 91 99124 8 <br /> Ch <br /> ,zN)mthreeene yg&g OPb) 170 4 7aft4 89 50122 9 <br /> Beennm@)Ruoanthene p6Ag0Pb) 170 4 a97 b 82 bl" 9 �. <br /> BenmWDuomamen. pglkg(nPb) 170 4 90 88 55135 9 <br /> BmmWPYreae p&gOpb) 170 `5 85 92 49.129 7 <br /> Indma(1,2,3ad)Pyrene pe/kg Ob) 170 4 a7 96 97132 l0 <br /> DAenm(a.h)an r ae nAg Npb) 170 4 91 IN 97-136 IO I' <br /> BervmN.h,ODerybno pghg(ppb) 170 `5 88 97 26132 ]0 <br /> m�The analyte wax not deNuednmeor mareofWe dupliran malyses.76exefore,Wcuntion of <br /> Ise RPDmno[epplicahle. - <br /> 22 23 <br />