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FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> - -` - ENy1ROFM¢ ALCt0itA8TS ENVRtONMINfALCBFAISTS <br /> �t Analysis Fax PNA Compounds By EPA Method 82900 SIM - <br /> _. Date of Report IU32/03 <br /> CRmt6 pinM: Method&lank Clket Ommatra Covmlkecs,Inn Date Received: 10127)03 <br /> Dak Received: No[Apphcable Pzolrt 501I.M.FMISIONS Project: 5011.003,F&BI 310245 <br /> DoleExkeck& 1D034U LabH); .62011152 <br /> T.r^_ Date Mayzed: ItwtX1 - Dak PRe: 110596D - QUALITYASSUFANCERESULTSFROMTHE ANALYSIS OFSOIL SAMPLES <br /> Mew: Sol taus rot GGA FOR TOTAL PETROLEUM HYDROCARBONS AS CRUDE OIL <br /> U k, ughg(ppb) - 0,e..,. YA USINGEPAMET11OD8015M <br /> Lower Upper <br /> S nagetee: %Aerwery L'wif Limn Labonkry Cade:310235-0I(DuP6kk) <br /> __ Mthrmenedl0 86 53' 92 Relative PeacenL <br /> s" BevzMa)mtGattne.dU _116 & 100 Reporting Semple DuPRmte Diff.renm <br /> }P} _ Concenhaemo: Analyte Unita HaugRaul[ ( t201 <br /> 31 Cvmpomdr ughgtypb): Crude OR We(ppo) 40 40 em <br /> N phtlmlane 4 <br /> Acenaphthylene 6 Lnbommry Cade:91029601 @Sahiz BpJe) <br /> MmnphNme 4 Pexm[ Percent <br /> Pluerme 4 - Reporting Spike Semple R%7 Ii M Aceepria RPD <br /> i' Phewnth.na e.5 Mai U' level ReauR h15 MSD Crikria 63mi[29) <br /> Arehairmu 4 - Crude On wg tepee 500 W 100 51 65.186 6 <br /> Flumavthme 4 <br /> 4 <br /> 8 eo—fluereve Labomkry Code:Leborakry CovwlSwPle <br /> CM1peen. 4 Pemeet Pemeet <br /> Henm@)Duoraethene 4 Repmtivg Spike R—iixr Recovery ArrePkere RPD <br /> HmzARluoranthene 6 - Anal Un'k ]sal LCS IASD C45terie (Limit4,71 <br /> Renm(a)plo 4 bode OH Yglg@PW 500 106 109 65135 9 <br /> ]ndeno(I0)..,roree 4 <br /> Dtheem(ath)anthrecene 6 <br /> �. BmzMg,h,Operylene 4 onear . <br /> '. " nm"Disnot Vplieno[de[mtedie morea[the duplizak amlysea'ILerefure,ralcuktwno( <br /> the RPD k not aPp4aeble. <br /> I: <br /> 3 <br /> 3 8 9 <br /> FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> ENVRtONSfENTAL CHEM(SfsENYRtONMENTALCREM s <br /> Dataof Report 11/12/03 Dmcif RepOet L1/12103 <br /> - Datelteceive& 10/29/03 Date Received: 1027/03 <br /> Project 5U11.003,F&111310215 Project 5011.003,F&BI 310245 <br /> QUALITY ASSURANCE RESULTS FOR THEANALYSIS OF SOIL SAMPLES - QUALTTYASSURANCERFSULTSFORTHEANALYSISOFSOM <br /> FOR VOLATILES BY EPA METHOD 8260B SAMPLES FOR PNA'S BY EPA METHOD 8270C SIM' <br /> k" Luherakry Code:31023541(Duplicek) IsMrakry Cade:310245-02 p)up5mk7 <br /> Relative Parsat ' Relative Porten[ <br /> lloati g Sample Duphrak mi. R,Rortio6 Sample DuPRkk Di&renre <br /> ( MeI Unv. Rwlt Remit 03mi[20� Mai Units <br /> Aaul[ n...[ (Limit 201 <br /> Benzene pg1B@pea ..005 9.005 NapM1ttulene wrg(ppb) 4 4 <br /> nm <br /> Tolume. Ric(pp.) <br /> 9.005 9.005 ( nm - AcevaPM1thYleee pHhg@Pb) 4 4 <br /> .� EthYlbenc a Pet(PP.) .-.9.005 9.005 n ArenaYhtheee mft(ppb) 4 4 <br /> mP'X1kne <br /> Wit(pp.) 9.035 900(ei - morce.a M&C(Ppb) 9 4 <br /> 9 <br /> o-Xylme We(pp.) 9.005 .005 sw Phenth <br /> aareoe i,ghg(pPb) 4 4 <br /> nm MtM1racene pWkg(pPb) 4 4non <br /> 'i. PluonnWene pghg(ppb) 4 .4 <br /> Labora.ry Code:slum-0t(mLtria Sp@e) PYrme p fteppb) 4 4 <br /> .a Pasant Percent Hena(a)mlhramne pghg(PPb) 4 e5 <br /> �" RepmovB SPhe Sample H.wery Pawery A.epkvre RPO Chryaene pghgWb) 4 4 <br /> Mel U Isel 1 MS 3dSN Crikria ([imie201 lien.@)Ouarmdi— Yg1k6@Pb) 4 4 <br /> ]Ynune - pg/g(ppm) 0.05 9.005 102 106 '16190 4 Renzo(100uomnthme pghg@pb) 9 4 <br /> - ]chime iWg(pPm) 0.05 9.005 - 703 110 700.130 6 Nnm(a)PY.ee 'pghg(ppbl 4 4 <br /> Ethylbe=m _ pgl6@P.) 0.05 9.e05 98 105 90190 7 - Indeno(1, aodpyrene pglkg(.ph) 4 e5 <br /> #; mOXykne. <br /> V,(,p.) Rce . ccxi 100 109 96130 8 Ddunzo(e,)amthreeme pghg(.pb) 4 4 <br /> �^ o-%Ylene yB/g(➢Pm) 0.05 9.M 9R 105 90130 7 B .(gh,aP.ylme pghg(ppb) 4 4 n. <br /> (shoretorY Cade:910245020dahia SPHe) <br /> ISMmkry,Code.Labommry fhnwlSamPle Percent Pert.[ <br /> Perteo[ Pemxnt - Reporting Spike' SamPla Bravery Hemvery Aceepunm RPD <br /> 2 Rep ff 8p&e R MU RemMery hx' .a RPD J U Le+I Peaul MB MRD Criteria (Limitm <br /> Yr- Aodvte U' Iev l [.CS LCE Criteria (I.ivd[20) - Naphthalene K&g Wpb) 790 4 83 85 66117 9 <br /> Br.-n. pglg(pp.) 0 <br /> .05 102 101 I= 2 Acenaphthylene pghg(ppb) 190 9 09 Re 5 is 3 <br /> Toluene pg/g(pp.) 0.05 10999 70190 4 Acenaphthene pghg(ppb) 190 4 RB el 59-114 3 <br /> Ethylhenzeve pgk(ppm) 005 98 95 70130 2 Fi-.e pghg(pple 170 4 82 85 61-119 4 <br /> Y• cop-Xylpeg 11-pre) 005 100 97 ]6190 2 Phamnthrene pghg @pb) 170 4 W 85 SL122 2 <br /> o Xxlene pg/g(PP4 0.05 He m 70130 2 Mthrmme pghg(pp6) 170 4 78 BO 50116 2 <br /> C Fluorankene pghg(ppb) 170 4 92 94 52-im 3 <br /> Pyr-e pghgtppb) 170 4 93 05 49-124 2 <br /> 1y Benr(a)mthmcme pghg(ppb) 170 d 84 85 50.122I <br /> = m-7M1e analyk was va[deuctNinmeermom aftheduPRkk malyen.Tnerrbre,ralcu R000[ Chryaene lghg(ppb) 170 4 84 QB 4&121 2 <br /> Ne RPD uvotapplicable. &vm@)0—ffiena pglkg(ppb) 170 4 94 N 51144 2 <br /> Henm000uvmntheva pghg(ppb) 170 4 RR 91 55-185 4 <br /> 3— Bmm()pyreee pghg(ppb) 170 4 77 78 49-132 1 <br /> x' Indeno(I.R.9r9PYrme pglkg Ripb) 170 6 84 85 37.132 1 <br /> Dibmmp.M1)enthere neo,(Ppb) 170 4 M 89 37136 1 <br /> Beorafgh 7perylene pghg@pb) 170 9 82 84 28-192 2 <br /> v <br /> sheaHPD'.RPD isealyk was natdeta[Ninoeemmere aEke duel'rakarulyees TnexEore,dcu)atim of._ <br /> m[apPRubin , <br /> 10 11 <br /> 1- r, <br />