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FRBDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> ENVBtONMEtI'LAL(:FIDFIISTS - - ]]WHtONMENTAt CHEMISTS <br /> Anajysis Foy PNA Compaaode By EPAMethad8270CSIM Datadllapart 1)/14/03 <br /> COen[SemDle ID: Method Blank Came Ucmam C aaultaae,lac Date Received 10/24/03 <br /> Dem Beceivcd Not AppL Me Psojce SO1L009.F&01310]35 Psojeet:50Il.003;F&B1310235 <br /> Date Exmatee& ItwW _ lablD mb200.1152 <br /> f7 Date.Maly ck 1IM00 Data File: llasosn QUALITY ASSURANCE RESULTS FROM THE ANALYSIS OF SOILSAMPLES <br /> $ ' <br /> Mae— Bail Rumummc (:CMS3 FOR TOTAL PETROLEUM HYDROCARBONS AS CRUDE OIL <br /> uni. ug&g(ppb) Op®mr. YA <br /> ' USING EPA METHOD 8015M <br /> lmvec Upper <br /> : Sus tea: %Revery Limit Limit L canary Cod¢:310235-01(Dupliram) <br /> Mttmmneal0 P6 53 0 Nleme Pemvnt <br /> Bmw(a)anWcacened12 86 64 100 Re ,tivg Bamptu D.plimte Dee— <br /> . Comrenmatim: Mahn. Uvim Heeult Result (Limit201 <br /> Commwdsg&g(ppb) .. Cmde Oil peg(PP.) 450 b0 nm <br /> Naphthaline 45 <br /> A ,hthae 45 labamtmy Cade:91MRSO10Nemis SPae) <br /> hthenine b Pecans Pecan[ <br /> Fluare <br /> ' Flum¢ae. 45 RemrNne Spiky Sample Recovery RKgn Amepmnro PPD <br /> anfl hrene - 46 Malv[e= Uvila -.1 Rand[ M8 MSD Cri[erse (1-'m.. 01 <br /> Mthmmne b Crude OJ WK(plan) 500 b0 l00 94 64195 8 <br /> Pldorwthme 46 <br /> Pytu b <br /> chn'Nethra<me c rnaaryCode:fabmamry CmwlSample <br /> F' Be..cooBuocanthme b _ Perem[ Pereen[ <br /> Bmm(kRlwrmthme b - Retorting Spike Ree'wery ]lawery Amrymnro RPD <br /> An.l a Unit Cate, LC9 Me tcn tis (Limi 0) <br /> Benzo(e)Pymne 45 Crude pd IWI(PPm) 500 106 103 65-135 3 <br /> _.. IndmIXl,2.9.NJDYrine 43 <br /> nihmm(a,Wwthncena b <br /> BenWg.R,Jpmlme .b <br /> '3 aelPI)wcAt,pl mtderxmdivmammine afthe duplicamwilysee.34erefnm,celculetiov of <br /> the RPDuao[wPeceble <br /> �J. <br /> e 9 <br /> FRIEDMAN&BRUYA,INC. FR®MAN&BRUYA,INC. <br /> ENVR1O1A4N'FAL CFBIIRSIS ENV1RONhMIIYALCHEMISTS <br /> ,. Dateof Report IDI4A03 Date of Report: 11/14/03 <br /> Date Received: 10/24103 Date Received: 10/24/03 <br /> l Ptoject 5011.003,F&BIS10235 Ptojeok 501L003,F&B1310235 <br /> QUALITYASSURANCE RESULTS FOR THE ANALYSIS OFSOD,SAMPLES QUALITYASSURANCE RESULTS FOR THE ANALYSIS OF SOIL <br /> FOR VOLATILES BY EPA METHOD 8260B SAMPLES FOR PNA'S BY EPA METHOD 8270C SIM <br /> tebmemry Code:310295-01(Wp0mm) Lebommry Code:310245ffi(DuPRmm) <br /> Re IsWtrent.n[ RdDffe ente <br /> RemsBne Sample Duplicate pi8'erence Papaatin6 Sample Duplimm DiBerence <br /> Malvin Uaim ResultRmu11 01 Melvin Uvim Amutt Aeaul[ (Limi[IDI <br /> :r Bmmva p6(g tppm) -- b.WS NaDhthalme yghe @Pbl b 45 <br /> Totame pglg tppm) ¢0.695 m035 nna MenaPhthylane pg&e fpDb) b b <br /> EthYlhevene we fppne) m005 m,D35 an, AcenwhOme pg/kgo b) b 6 <br /> ?` m,p.XYlme pglg(ppm) 41.005 <tmnn F)uoane pykg(P0b) e5 e5nm <br /> o-XYlme K"(pl.) �OA05 b.005 nm Phmantbcene PYkg(DPb b b <br /> Mthca pg&g(Dpb) 45 4 <br /> Fluocanthme <br /> laboramry Code:31ou"iliat spa.) Pe wAg IPA) b e5nan <br /> Pemevt P-1 BeatWanthmaene nft fppb) b r5nm <br /> '�. R¢Pnr[wg Syike S—ple Rzwery P ., A ,,aanro IED Chryaene pP&"tb) c5 d <br /> Mdvm Unim Leve) R l MS MSD C' ' (Lim'21 Benm@1Duvmathene Wk9(ppb) b e5 <br /> Bemene p81g(Na') o,a5', mam am lbs 9a-130 4 Banmtk)Bum.a(hene ng g(PPb) b b <br /> 3bluine K"(PPW 0.05 X0.005 103 1I0 ]0.130 6 BmaIXa)pyrene pg&g(ypb) b b <br /> Ethylbemene K"(ppm) 0.05 b.005 m 105 ]0.130 ] lndesm(k2,3,aop nene WNg(0pb) 4i bnm <br /> m,P Xylene We(PP.) 0.0.5 b.o05 100 107 70.1308 - nibenm(a,h)anthmara pg&,(,,b, b e,5a. <br /> a-Xylene W9(PP.) am '0.005 98 IDS ]6190 ] Bevo(g.hAperyime VeA6(ppb) b 45 nm <br /> Lebammry .:31024402 Qdalru Splke) <br /> Iabocamry Cade:L nnaaryC entsamPle N-1 Pemevt <br /> Pecan[ Percent Reporting Span Sample R>awery Pecmery Am tante PPD <br /> Rryortiae Spae Revery Recovery Accmmnce RPD -9111M, <br /> Melw Unim lavtl Aesul[ MS MS Cri lL:m'201 <br /> Analyte pyre Level LCS LCSp Criteria (Limit 20) Naphthalev¢ Kft(ppb) 170 -� 83 SS W117 a <br /> Benaene pg18(ppm) 0.05 IM 101 ]9139 2 AcewphtIntne "ft(ppb) Ito 87 90 59115 3 <br /> ,5 Tolume Vera tppe0 a05 103 N ]0.190 4 Menaphthene Pg&g(ppb) 170 45 88 91 59.114 9 <br /> EthYlbenrin0 perg NPm) 0.65 00 95 70-130 2 Flumene K&C(Ppb) 170 cb 82 85 61-113 4 <br /> mp-XYlme n"NPm) 0.05 100 W 90.190 2 Ph—daene K5,9IPPB) 170 45 84 85 51-(22 2 <br /> o Xylene - ypg on 0.05 I00 90 )0190 2 An m . Kota 1ppb) 170 <5 70 80 50.116 2 <br /> Pluomnthene pghg(ppb) 170 ei 92 N 52124 3 <br /> Bena<e)mthmcme p41kg(pPb) 170 b 93 95 49124 2 <br /> Lk _ K&g(pp5) 170 45 84 m 50.122 1 <br /> the UID ewlymwaenotdeMlatin memmaceafthe duplimm milyam.lfi¢regire,mkula[iond KA9(ppb) 170 46 04 S6 121 2 <br /> the BPDunot applicable. CM1rysine 49 <br /> Itnte- )auonnthese pghg(ppb) 170 c5 94 96 52144 2 <br /> Benmp'Jnwmnthme paha tppb) 170 •5 89 91 55135 4 <br /> pg&g(ppb) 170 b 77 78 49128 t <br /> dena(1.2,3d1pymne yghg(pto 170 b 84 85 37-I32 I <br /> S Vffnnm(a.h)anthrerene pg&g(ppb) 170 45 N 89 32136 1 <br /> ��SSaa Benao(g.h,Jperylene Kate 1ptb) CO <5 82 84 M132 2 <br /> -7TeenelymwU=tdelx4dinmeormmeafthedupl4 mre ysm Therefor,m uletiond <br /> �: Na RPDu not applicable <br /> 10 <br />