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FR®MAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> 3) ENVIRONMENtALCHQASn ENVIRQNMFNTALCHEMISTS <br /> as # Analysis For PHA Gompooads By EPA Method 8270C SIM _ Da4o[Report: 11114/03 <br /> i Date Received: 10/30/03 <br /> �- Date Sempk lD: Method Bknk Clinic emmaeria C.s31ffiW Iv¢ project 5011.003,F&BI330306 <br /> Dem Received: Nm AppBubla P m- SOIL0-1152 I3L0306 <br /> Date Ertneud: 1D 3 7M 1D: b2 03-1152 <br /> Dau Analyzed: IIW)3 Dam Fila:. MIND QUALITY ASSURANCE RESULTS FROM THE ANALYSIS OF SOIL SAMPLES <br /> bdntr Ena Inetzument ccM - FOR TOTAL PETROLEUM HYDROCARBONS AS CRUDE OIL <br /> u¢im: vg/kg(Ppb) Opener. YA USING EPA METHOD 8015M <br /> /axe[ UPp++ <br /> Surmgatea: XR Loot Limit IobozemryCade:3L0295-01(nup4mm) <br /> Mmrere¢ed10 86V3 53 92 Iklativeenoe <br /> B mMa).Ouama¢dl2 86 64 100 Rem[ting Sempk ORosult gunk re <br /> Cmcenmatim: Malvee Un:. Result Rnult ryimi[201 <br /> ont <br /> .'Qnnp0000nchr ug&g(ppb) Ltude OD Kg(pp.) d0 e50 vin <br /> N PhthO. 5 <br /> Amamhthylme 6 Laho[aroty Cade:31023501(drir Sp&e) <br /> MempM1Wena - I.., Persat <br /> Fluo[eve 6 llepn[Ung Spite SamP4 Retwery Bxa+ery Meepmnea RPD <br /> Phenen0unic W Melvin Uniu Laval Rerult MS MSD C[imria (mit20) <br /> Auttracen. <br /> e5 Cnde Oil Rig(ppm) 500 e50 IN N 65195 6 <br /> ch... <br /> BNanN[ezme c5 L6nnery(.`Nc laMnep Canlml8ample <br /> Chry - <6 Percent Pert.[ <br /> BevmW)0ummthe a �b Repotting SP&e Recovery Recovery m <br /> Aeepnoe RPD <br /> Bmm(k)Ouonuth a x5 Melvin Units Lmel IM 1C 1) C¢teme (ka%) <br /> Bmm(e)pyam e5 C[ude oil Kg(pp.) 500 IN 103 65135 3 <br /> [dmo(12,3e'd)pyrene <br /> 45. <br /> nOvaza( h)a¢W[ecene c,5 <br /> Be Wh,Operyle a �5 nm-7hestoo wanobt,. «udmmeo[moripfNe du Lem oval <br /> &e APDumt.PRcebk. P yzec TTerefon,nkWetim of <br /> E3 <br /> 1.' 8 9 <br /> FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA;INC. <br /> EdV9BONMENFAL CIiEh1 s ENVIRON VtLCBEMLSFS <br /> 5 DoloodRePert 11714/03 DateofReport: 11114/03 <br /> Date Received 10/30/03 Date Received: 1050103 <br /> Ptoject 5011.003,F&BI310306 _ Project, 5011.003,F&BI 310306 <br /> ' - QUALITY ASSURANCE RESULTS FORTHEANALYSIS OF SOIL SAMPLES QUALITYASSURANCE RESULTS FOR TILE ANALYSIS OF SOIL <br /> '- FORVOLATILESBYEPAMETHOD826013 SAMPLES FOR PNA•S BYEPAMETHOD 8270CSOI <br /> I rototy Code:nam w M-pOnte) LbotemryCade:3I0245A2(Dupante) <br /> Relative Pertmt Rek Ea roan <br /> Aeporting Samek Duesmm DiRecence _ Aepmting Semple nR000lte DiHenme <br /> on <br /> M Iym goo 4ON Remlt (Li om Melvin Uvlm R¢ml[ Aenit (Limit 201 <br /> Henze. - pglg(ppm) m.WS <.095 Aonn,hlme yg&g(ppb) 4 4 <br /> ]flume pdg(pp.) A.o05 ol) 0m MenaphWylene mat(ppb) 4 45 <br /> EWy@even¢ pg/g(Ppm) AWs <0.005 iIu..n0,ene yg&g(Ppo, �-`� 45 <br /> "'. mtrXPlene vz(ppm) 4m m.N6 Fluorine pghg(PPb) 4 4 <br /> u%ykve vg/e Wpm) A.005 N.WS nm Phenanthrene pg&g(ppb) r6 5 <br /> Anthracene pghg(ppb) 4 o�5 non <br /> Gbmamry Cade:310995(&Wrir Spike) FluoamsNene yg&g Wpb) 4 e5 - <br /> ' Pemmt Henz(elantM1ncene m&g Wpb) 6 e5non <br /> Reporting sp&n Snmple Ret m A ymma Mr.. pg&g(III) 6 c5 rum <br /> "'- - Mdvm U,um Imd Result MS C64nn BenmW)n...tb.e Wag(ppb) 6 `5 nom <br /> Be— p lg(pom) am oftm 70 70130 B.io(k)Rvormn0,me MAC(1pb) 6 s5 <br /> Tdu.e ",(Ppm) 0.05 �m 82 70.130 Bo.r,N yrene Mar(ppb) 6 c5non <br /> = E[hylbenzene W'(PPm) 0.05 x.005 77 70130 Indmo(1,2,9cd)PYreae R&e(ppb) <br /> .., oo P-Xykne V C.P.) 0.05 X0.005 76 Mim Dib.zo(.A)enNnnne &,(ppb) 4 c5 <br /> ,Xylene peg(ppm) ,0.05 a).005 74 76lm Beveo(g,h,,ml— pg&g opb) N e5 nm <br /> / IaMneryCWe'9102dS02(bmtrSx SP&e) <br /> lntanmry Cade:Iabonmry Cmtld Sample Pemen[ Pe[ceer <br /> t. Percent Pecten[ Reporting Bpike Sample Remwery Recovery Atcepmnce RPD <br /> Repoctiv6 Spike Recovery Recovery Am Prance 'Keri M 1 Uv' Lev 1 Resin[ MS MSD Criteria (Uxnit20) <br /> '. <br /> Anal'. Unite Level LC$ LCSD Crimrk (LLvit20) - N30M1tM1dene pghg(ppb) 170 c5 89 85 58-117 J <br /> 1. Benzene py/g(ppm) 0.05 BB 89 ]6190 1 Ananephthyk¢e R&g(ppb) 110 ti 87 90 59115 3 <br /> �' Taluena pg/g(ppm) 0.05 m 0 70.130 2 Acenaphthene pg&g(.pb) 170 e5 88 91 53114 3 <br /> Rffiy me pft(ppm) &05 92 94 70.130 1 <br /> zFluorine pg&g(pph) 170 c5 B2 85 61-119 4 <br /> m pXylene nt C.P.) 005 98 N MIN 0 Phemn&rene pg&g(.ph) 170 6 81 86 51-122 2 <br /> o-Xylene mIg(PP-) 0.05 95 m 70.130 1 Mehncene pgAg(ppb) 170 c5 78 N 0.116 2 <br /> Fluonnthene pp/kg(ppb) 170 o5 m 94 52124 9 <br /> nm TTeemlym win not defecmdmmemmare of thedupLmm mdyan.TTereS¢e,mkuktimd Pyrene pg&g@Pb) 110 c5 N 95 4MM 2 <br /> Be-Nanthnxne pWkg(ppb) 170 o5 24 m 50.1221 <br /> S.L the RPDmnot apP6nble Chtyzene pg&g(ppb) 170 e5 m 86 48-121 2 <br /> Benzoo)RuozanNem K&B Wpb) 170 e5 N 96 62-IM 2 <br /> q BevaNfluvnntome pg&g(ppb) 110 4 N 91 55135 4 <br /> fi _ 0mea(a1PYnne pg&gopb) 170 6 77 T6 4%im I <br /> ! Nd.o(L2,9ad)pn.e pg&g(ppb) 170 e5 89 m 37-132 1 <br /> Ben,Omn me ne yg/kg(ppb) 170 e6 BB 89 37-136 <br /> �- pPkg Wpb) I70 6 J2 B4 2$132 2 <br /> m sndym win na[dememdkme oc ma[eo(the duo Wae emlyua.TTetekre,ml Wntionof�. _ the RI'D RPD is na[epplinble. <br /> y 10 <br /> _ _xv- <br />