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FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> ENVIRONMENNfAL CHEMISTS ENVBIONMEWTAL CHEMITIS <br /> Dmbedlto rt: 11/14103 DateofRepc= IU14103 <br /> Date Received: 10/24/03 Date Heceive3 10124103 <br /> Project 5011.003,F&BI310237 p<Oject: 5011.00%F&B1310237 <br /> QUALITY ASSURANCE RESULTS FOR THEANALYSIS OF SOIL SAMPLES QUALFTYASSURANCE RESULTS FORTHEANALYSIS OF SOIL SAMPLES <br /> FOR VOLATILES BY EPA METHOD 8260B FOR VOLATILES BY EPA METHOD 8260B <br /> Laboratory Cade:310=4)4 Dupl'vate) Lob omry Cadre 3I02860l(Dm mm) <br /> Relative Pacevt Rdamre ener, <br /> Aeportiog Sample Oup5m4 DiRmeme Repores Sample Dupecam mmit <e <br /> Malele Ureic, R Ws Result ry nor Immeme lln'm Aemlt ReauLL Q.uvit 210 <br /> Bmzma Wx WPnil 9.ua5 x0.005 Remem lwg Wpm) <..005 9.005 <br /> mMe'Ho <br /> Tblume W/g WPm) 9M5 9.005 Toluene pgt(pp.) '0.005 9.005 <br /> EWyBwamne wg(Pm) 9.005 9.005 mP-Xylnzene yg/g NPm) x0.005 <br /> mXylrr eve pwt(P.) <()W 9A05 mX Io me pgrg(pp.) 9(m 9.005 <br /> a%Nene pg/g(Pm) 9,005 A005 � nm o-%Ylme yg/g Wpm) 9.005 9.035 nm <br /> Labonmry Cadre 810W7 I(h%emx Spike) Pertent Pemevt ImMramry Cade:3102364)1(Merrie Spiko) Pemmt Percent ., <br /> ReporCvg seilee Semple Remveq Regie ey %mep- UD Imerung Spike Sample Hennery Hem+ery Arm Amore RPD <br /> Melvin Units ]mel Remi[ MR 3150 Crfmaie (Dmit2m Malvte UmAe Level Reml[ MS k15D Criteria (f.imi[2(1) <br /> flemorem W9(pm) 0.06 9.005 IN I06 76130 4 Benzene <br /> 'Flume IW9(19.) 0.05 9()W IN 110 70.130 8 V"Wpm) OAS 9.00.5 IN IN ]0.130 1 <br /> EWyR,emme yg/g(pp.) 0.05 9.005 M 105 76190 7 'Flume yg/g(ppm) OAS 9.005 104 w 7(1IW 9 <br /> m.P-%Ylme pwg WPm) 0M 9.005 IN 107 74130 8 m.P-Xyncene pg/g(ppm) 0.05 10005 93 97 76190 6 <br /> o-Xylom ywg(ppm) ODS 10.005 98 105 70.130 7 p-Ieorm a It(ppm) 0.05 9.005 N 94 ]0.130 5 <br /> o-Xyleno yg/g Wpm) 0.05 9.005 9o- 94 70.130 6 <br /> Lebamemy Cade:harem,Cantml Sample law.,Code:I mmry Control Semple <br /> Pmmnr Pammt Pemeot Percent <br /> Repmmng $Pike Recovery Rreemw Aremeanm RPD Repar[wg Spike Remvem Rerovvy Ammtaam RPD <br /> Mdy[e Imes level LCS IMD Crimria (I.wdt20) Milvee Units Levd LGS I.CSD Celle^, (Limit 210 <br /> Benzene pg/g Wpm) 405 102 101 70130 2 Henaeneyg/g WPB 0.05 IN 99 70.130 1 - <br /> Toluene pg/g Wpm) a05 103 99 70130 4 Tolueve <br /> Erhy0vvmne vwg Wpm) 0.05 w % MIN 2 Eehymenaem Wig(PP.) (IN 99 M 70.190 1 <br /> cap Xylene M[9(PP.) 0.05 IN 9'I MIM 2 m,P--Xymm wigWpm) 0.05 IW 102 76190 2 <br /> a-Xylene nl WPm) OAS IW 98 7o-130 2 o-Xylme pg/g Wpm) 0.05 100 N 70.130 1 <br /> me-Ile murlym oven.deteeted in me or dWe dupummamlysm.Tlemtoce,Gelml]m¢of <br /> me no avelym roes not dmeemd Sv me oc mom drhe duptmte mWyrM Them6ce,mlmlemn of Na RPDisme,ptreble <br /> the RPDmmrmp5mble. <br /> 20 21 <br /> FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> ENVRtONb>ENfA CHE BSTS ENVRtONMEYIALCEgARSTS <br /> DateafR wt,. 11/14/03 DmteofHepovt 11/14103 y <br /> Date Received: 10/24103 Dere Received: 10/24/03 <br /> PmjeM:5011.003,F&BI330237 Project 5011.003,F&BI310237 <br /> QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OPSOIL QUALMASSURANCE RESULTS FOR THE ANALYSIS OF SOIL <br /> SAMPLES FOR PNWS BY EPA METHOD 8270C SIM SAMPLES FOR PNA'S BY EPA METHOD 8270C SIM <br /> Iaboramm Code:3102/542 Mupleale) IabammryCade:labmamryCovtrd5emple __, <br /> Relative Parrem[ Pemeret proem, <br /> Reporting Sample Duplicate DWer. Reportiag Spike Ammmy Remiery A<em. RPD <br /> Malum Unica Result Reuh (L 2% d lm' <br /> m ]mel LCS LGSD Criteria fl imi[Nt <br /> NePuthalme yghg(ppb) 4 <5 NephUWena yghg Wpb) 170 S6 BD 6&121 4 <br /> Menaphtltyleme yghg(ppb) 4 4 (omphthyb:ne yghg(ppb) 170 89 93 54.122 4 <br /> MemphWme n&g(ppb) .4 4me Ammphemrrm yghg(.Pb) 170 9s 95 6&119 2 <br /> Fluorme pykg(ppb) 4 4me Somme yghg(ppb) 170 N 91 57-IM 2 <br /> .Phemothrme pghg(ppb) 4 4me Phmmvthmne pg&g(ppb) 170 87 M 57-121 1 <br /> MNrmene pghg(ppb) 4 4 Mtl rmre yghg(ppb) 170 79 R 41-I26 5 <br /> FluvmoNrm pghg(prb) 4 4 Flmomt)mm pg)kg(ppb) 170 N 97 54-12] 1 <br /> Pyrene pghg(ppb) 4 4mor Pyrene yghg(ppb) 170 99 M 56123 0 <br /> eme(e)mmuaem. yg/kg(ppb) 4 4nor Eem(e)enthre[ene yghg Wpb) 170 92 50.124 3 <br /> ChrI m, yghg Wpb) 4 4nor Clity a pglkg Wpb) 170 N 92 51.122 8 <br /> Hee-O)Ouomvthene yghg(pb) 4 4 roor pghg(1pb) 170 N IN 44149 2 <br /> lInm000mrm,lrene V2hg(,rPb) 4 4nor Revm(MOumenthme pghg(ppb) 170 99 98 52-140 5 <br /> fIm.(e),Mrm yghg(,pb) e5 4` me yghg(pPb) 176 72 80 42129 11 <br /> lodmo(1,2,3edlpymm yghg(ppb) 4 o-5me Indma(1.%3 dbyrme pghg(.pb) 170 92 94 4&184 2 <br /> D3enm(a.b)mffim,me yghg(,Pb) 4 4me Dilmm(gb)mOmmne yghg(.pb) 170 97 I00 49136 8 <br /> Bemo(y,b,OPerylene yghg(ppb) 4 4 me Henm(g,bApmrlme Vghg Wpb) 170 N N 46134 s <br /> . . I r mryCade:910245-02 Qdehii8pike) --- <br /> Percent Percent - <br /> Reporeing Spike Swpla Recovery Recovery AmroWm RPD <br /> Malme lkg0 Ica 1 H 1 DT M$ C R' m <br /> NephNelene ygUnier ) 170 4 89 85 6611] 9 <br /> Amuephthylene yghg Wpb) 170 4 87 50 59115 3 <br /> Acenaphdrene yghg Wpb) 170 4 N 91 59114 3 <br /> Flumene pghg(ppb) 170 4 82 85 61-113 4 <br /> Phermtbrme yghg(Ppb) 170 4 84 M 51.122 2 <br /> Mthmceve yghg(1pb) 170 4 78 80 50.116 2 <br /> Fluvrmt8ene pghg(ppb) 170 4 M 94 52124 3 <br /> P omem0ve<me yghg WPb) 170 4 93 95 49124 2 <br /> Chmame yghg(ppb) .170 4 BI BS 601221 <br /> p9hg(upb) 170 4 84 86 46121 2 <br /> Benro(b)Duo[mrhene pykg(ppe) 170 4 N 96 52144 2 <br /> Henm(y0um-thme pghg(opb) 170 4 N 91 55135 4 <br /> Henm(e)pymne pLkg(ppb) 170 e5 7] ]8. 431981 <br /> Indem(1,2,3Wpmnyu yghg Wpb) 170 o-5 84 85 37-132 1 <br /> Dfbenm(e,Nanthracene pghg(ppb) OO 4 N 89 37.136 1 <br /> Benm(g.hDPerylene pghg(ppb) 170 4 82 M 25132 2 <br /> -no emlyte roma nordeem Orlin one or more tithe duplimre malyeu.7Terefoce,mImIrrim d <br /> the RPD is vot apphrable. <br /> 22 23 <br />