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- FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. <br /> ENYBiONMENGLCEOihBS[S ENVBtON AL CHEbUSIB <br /> }.; Aaalydo For PNA Compomdv By EPAMeNod 82700 SIM DaIrofltepact 1N2W3 <br /> �:_ Client Semple ID: mcM10 Blink CRmc Germanic Conaulmnn.Inc Date Received: 10127/03 <br /> Dam Recebea: rvnr AppSnNe- Project: WILN3.P&B[3I0246 Project.5011.003,F&BI 310246 <br /> D.Eatrnrre3 IUWAXILeb ID mbN105 <br /> ' <br /> Door Avly ak ull - - - Dau File, IIIN1.O - QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF SOIL SAMPLES <br /> U=: Sao Ivdnmr. OCMS3 FOR VOLATILES BY EPA METHOD 8260B <br /> 1' U n: ughg(ppb) Irepre YA <br /> I—er Upper <br /> Swmgatrs: %Recver, Lmut umlr L minty C°dm 3102 01 Meplimm) <br /> Anthracene-dl0 73 44 113 Hehtive Pecevt <br /> i Renw(e)milu—e-d12 81 65 l94 Bepvating Sample DuPlinm OiHereme <br /> Cmrmmaoom M°lvm Udn Peaul[ Result (I.imit2O <br /> Compounds: ugag@Yb) Berens pg/g fppm) 90N 9.005nm <br /> Toluene pg/g fpper) <am 900.5 nee <br /> ' NephNalene - b - ErhyRencrne pglg(pre) 900.5 9005 nee <br /> ""IArhylane b m.P'XYIene Rlg(PPm) 9005 9005 <br /> MevephWm9a <br /> a b o-XYlene P9kk-Paa), ws 4015 noo <br /> ere FE sorer 4 <br /> Phmanehnve 4 - <br /> i-":_ Mthraeene b Labvnmry Cade:31023"1(Matix SPae) <br /> FluonnNme 4 - Percent Percent <br /> Pyrene 4 Repeating Spfle Semple I eery R ery Acceptmee BPD <br /> ,, Henz(a)mrhreeme 9 Aerl. Unim Levd Iurerit im MSD Coterie Od ,= <br /> S ' (hryseveBmvne p i"pere) am 9.015 IO2 IN 70.130 1 <br /> 7 Benm@)Buomuacac b MA... We(ppm) am 9.015 IN IN 70.1&1 3 <br /> Benb(kµluorevtM1me b EYM1ylben a pg"(Ppm) a05 4.AN 93 97 76130 6 <br /> i Henry 4p rene b m p Xylene pg/g(ppm) am 4.015 N 99 76130 6 <br /> maeno(1,2,sagpyrene 4 o.%rlma We(pper) 0.0 4.as 90 M 7MM s <br /> D3 zoo.h)mrhncene �5 <br /> Bmm(&h.werylme 4 <br /> Lebonmry Cade:Leboramey Cantel Sample <br /> .. I: Peon[ Pemmt <br /> Hepecec4: Spike Bemery I m Aeeprmce RPD <br /> Malvin Units I el I.CS LCSD Coterie pAreil20) <br /> Bmame Pg"Pm) 0.05- IN 99 70130 1 <br /> - Toluene Rig(PP.) am 90 97 76130 2 <br /> py 5NY@eneene pglg(,pm) am % N 70.130 1 <br /> ._ mp-XYlma <br /> wig(pp.) am 1N 102 76130 2 <br /> 1 uXylene pglg@pre) ON 1N N 76130 1 <br /> m-TM1.mdYm wunudememdm meofma aap5un melyem.TM1ererore,wraBtimd <br /> P'- the RPDmm[apPWahla <br /> 3 <br /> 16 17 <br /> FRIEDMAN&BRIIYA,INC. FRIEDMAN&BRUYA,INC. <br /> - ENVIRONMBNCAL'C'IffMI5T5 ENVBIONMENTALt1IDHISfS <br /> i-, <br /> -DabsofRepoct lVZU03 Datevf Report: 1121/03 <br /> Da[e Received: 1027/03 Date Received 1027/03 <br /> Project 5011.003,F&B[310296 Project 5011.003.F&BI310246 <br /> QUALITY ASSURANCE RESULTS FOR THEANALYSLS OFSOM QUALITY ASSURANCE RESULTS FOR THEANALYSIS OF SOIL <br /> SAMPLES FOR PNA'S BY EPA METHOD 8270C SIM SAMPLES FOR PNA'S BY EPA METHOD 8270C SIM <br /> I L cetr,cude SIM05-P5(OuPlinre) Lebo...Cade:LbonrmyC reel Semple <br /> Relative Pement Pecent Perch[ <br /> Reporting Semple Dup.^•r• DiBmenm Rmmtleg Spike Ree-., Recovery P rprmm RPD <br /> E.: Avelvm Unite Result Rea 1 201 Mdvre Unim Invel IZ3 LCSU Guinea Vreiem` —p—, pgag(ppe) 5 Nephaeme. pgag(ppb) 170 N 8B 5&121 4 <br /> ArznapM1Nylme - p¢ekg(ppb) b 4ner Acna0hN11me .IYag(PPb) 170 M 92 54122 6 <br /> Manephrhene pgag(ppb) 9 b Acenaphlenr KAg(ppb) 170 89 N 5&119 4 <br /> Pluoreve pgag@pb) 4 b nm Fluecene ,Ag(pple) 170 80 90 - 57-IM 5 <br /> .Phruv@eme Wkg@Pb) 4 bnm PheranNcma KAI,Q pb) 170 85 N 57-IM 4 <br /> AVWaceae Pr)kg Wh) e$ 4noo MNneene MAC(ppb) 170 76 84 44175 11 <br /> £Wocmthme pghg(ppb) efi <5nm Ru Gene KArg(PPb) 170 90 94 54127 4 <br /> Pyrene' ren <br /> Pyrene WAg(ppb) 170 N 95 56-IM 6� { ' Renr(°)m@eerme pghg(ppb) 4 e5pro pglkg(ppb) 170 85 91 50.124 8 <br /> 4 Cheyrene nerChersev° pg&C(ppb) 170 37 91 51-IM 6 <br /> Benm(b)Oe—ffi.e pghg(ppb) 6 bnee VgAg(ppb) 170 91 101 44110 4 <br /> Henm(k)DumaneAeve pgag(ppb) 4 4nue pgag(ppb) 170 86 92 52140 7 <br /> Benrv(a)pynne <br /> Mae(ppb) 9 c5nen Wkg(pb) 170 68 R2 42-IM 19 <br /> Indm°(1,23ccopyrcor pg&g(ppb) 4 e5on, lndeneU.2,3�Pyrme pgag Orb) 170 76 80 49.134 5 <br /> Di xe(e,htnW ene nag Wpb) 4 e5en D3enrot,h)mIlraeme p,&g(ppS 170 81 m 43136S <br /> Hmm(g.h,aPerylene pgae(PPb) 4 4 nen BeneMg,h.0peglene nag(ppb) 170 76 8l 46134 6 <br /> .{ Lboramy Code:31N0505(9anir Spike) <br /> Peemt Pcecv[ <br /> It Bp4e S. lo Remvep Rero+eey Arceptmce RPD <br /> Mdvn Uric Iavd Rea I MB MSD crioerch (Lm.201 <br /> NephrM1dme pghg(ppb) 170 b 81 85 56117 6 <br /> Areauphehylme �Wkg(plb) 170 4 M '89 5&115 6 <br /> }' -.e,@me pgA,(ppb) 170 4 m 89 59114 5 <br /> Fa <br /> pennnaume Aff(ppb) 170 b 82 85 61-113 4 <br /> Ph <br /> ph—cp e - nAff(ppb) 170 b 80 84 511224 _ <br /> r¢`ek FI—Mune m (Ppb) 170 4 75 M 56116 4 <br /> t 1jL pP/kg@pb) 170 b 86 88 52124 4 <br /> B vx(e)enNrerene PCag@pb) 170 4 87 91 43124 4 <br /> i:. pgft o,pbl 170 c5 82 05 50.122 3 <br /> c M&g(ppb) 170 < 82 89 4&12l 4 <br /> Bevin@IBuorentbene pgag(PPb) 170 4 N 98 62144 5 <br /> ;j Benkv(kplammrhme peag@pb) 170 b 64 87 MIS5 4 <br /> Bmm(°)pynne p&g(ppb) 170 b 7a76 49-128 4 <br /> g 1 Ivdma(1,2,3,cd)pyeen° pekg(Pb) l70 b 74 Tl 30.132 5 <br /> D@evn@,h)an@nrene wirg(ppbl 170 e5 79 82 87.136 4 <br /> Re^m(g.h,aP°rylene M&'g(ppb) 170 c5 75 78 M132 4 <br /> a <br /> theRPDulTD is dyer wee not dememd in vve oc mine o(lhe dup5mm e�mlpu.7beml re.ulwletiov N - <br /> � - mtepPRmbm. <br /> 8 19 <br />