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FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. ENVBt)NMUNTALCHEMISPS ENVRtON�bY1'AL C11EbIST6 Dateof Report 1120103 Date of Report IU20/03 ' Date Rectived: 1029103 - Date Received: 1029/03 Project 5011.003,F&BI 310287 Project 5011.003,F&BI 310287 QUALITYASSURANCE RESULTS FOR THE ANALYSIS OF WATER QUALITYASSURANCERESULTSFORTHEANALYSISOFWATER y SAMPLES FOR BENZENE,TOLUENE,ETHYLBENZENE, SAMPLES FOR TOTAL PETROLEUM HYDROCARBONS AS DIESEL XYLENES AND TPH AS GASOLINE USING EPA METHOD 9015M USING EPA METHODS 8021B AND 8015M L tvy Cade:3102i84N(Duplicate) Relative Peaent Lebpabry Code:Leha[uory CantmlSample i Repnm Sample Duplicate Doo[enu PeemPemmt S. Mel UdiG Penult Rnul[ (Lima 20 - ReWztng Spike Ifecwary Ocmrery romRPD ]kvzene pg/L(ppb) 1 1 0 MM Univ Ievel LCS LCBC D Criteri.a (Limi[= Toluene poob(ppb) <t <t nm Diesel pg/L fPpb) 2,500 too 104 7I-IRS 0 Effiyomzene ,&(ppb) 3 2 a r1-< X,4mev p,,%(ppb) 6 ea0- 155 G—om. pgh(ppb) <50 - X. S.. Lakammry Cade:Pnhoramry Cantil Semple Percent Passat pugs g Stoma Rew+ery ery &eaptanca RPD Malvte UNG Level LC$ RecovLCSD Criteria ffimit 201 3 Benzine pG( op" N 94 ve Tl.116 4 1117 Toluene M&Cpb) M 91 96 64126 5 EtbYlbenuve pglL(ppb) 25 92 66 64124 4 %ylenev not Qpb) 75 87 92 74121 6 GamSne no,(ppb) 1:000 M N 49.119 4 r '' m-The analyte wv cot deteebdinane ormv[eolWe dupScaG analyw.TTmefa[e,zakula0vv of '� t'.: rbc RPDGmtepP6vabla ' a TTaenNyte wavdetec[edeta lrvNiw Baan five times the deGetion limi6 The RPD.-Itseay �, vo[paw.ide c4liableiNormation vv tbevariab8ityafNoane)yeu e j . 3. 8 9 '-d FRIEDMAN&BRUYA,INC. FRIEDMAN&BRUYA,INC. ENVIRONMENTAL CHEMISTS ENVIRONMENTAL CHEMISTS � . Date of Report 1120103 Damof RePOK: 1120/03 5 Date Received: 1029103 Date Received: IOM9103 Project 5011.003,F&BI 310287 Pmject 5011.003,F&BI310287 QUALITY ASSURANCE RESULTS FOR THEANALYSIS OF WATER QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF WATER � . SAMPLES FOR TOTAL PETROLEUM HYDROCARBONS AS DIESEL SAMPLES FOR PNXS BY EPA METHOD 8270C SIM USING EPA METHOD 8016M �:. LabvamryCode:91075216 plata Spike) :S Pemenp Pee mr, labnnmry Code:Inbombry Contol Semple 5rce Gel _ Repvning 6 ,l Sample Pew Rmaery Am,.. RPD t Percent Percent M A.(V Level Rv0.1 70 MSD Cribria (l:mn.2p) PUnim Spike 1leics Pemvery AaePmia RPD Acampelene pglL(Ppb) 5 4.1 '70 70 70-IM 0 JJt(( MN2m M&(ppb) Level IN LCSD Criteria Limit YR AcenaPhthYleve IWI,(ppb) 5 4.1 71 70 70 IN 1 t!d Dimer pgh(ppb) 2,500 104 92 7}135 12 pcentaffieme nLopb1 5 4.1 75 73 70-130 2 Fluvave PgIL@pb) 5 4.1 75 71 70-IN 5 mfla [ane pg/1.(ppb) 5 <0.1 80 71 70130 12 ^ numanthe pp/L(ppb) 5 A.1 M 71 70130 11 Plumnvthme pe/L(ppb) 5 4.1 83 75 70 IN 10 Pyreve no,((eb) 5 <0.I M 76 76130 19 Bena(chnt5maene K&Npb) 5 m.l 84 76 76130 10 9 CM1ryame pgA,(ppb) 5 mA 83 76 70130 9 Benmp)Baomn0vne pVL oppb) 5 <1 M 73 70130 10 Benm(k10DOGnL1me pg2(ppb) 5 <0.1 80 73 76130 Benm( pg,Lpb) '5 .1 77 70 7 a(1,LII3d30 7 Ivdm ,10an v aocam n"pb) '5 4<0 M.1 56 78 701 130 9 the-k.M1Operylem, wo,omb) 5 10.1 85 77 76130 10 r. In mtm,code:Labambry Control Sample Pement Pemn[ y'. RepaKwg $p0[e oac,mry Reco+ery A aptanee RPD N Un"G Level LCs LD50 Criteria (Limit 20) NapM1RWeae pgh(ppb) 5 76 BO 70.167 4 Aanaphdt leve pgh(ppb) 5 8- N 65.116 4 Acenxotluma MIoppb) 5 83 N 76114 3 R.-mm no,op b) 5 79 83 86It3 4 Pbevandirene Pgh(ppoo 5 81 M 72109 3 3:. M—antimme no,Cpb) 5 91 93 66109 3 'f &- WLmpb) 5 N 95 75109 3 Benz(a)mNaceue n&(ppb) 5 88 93 52-120 6 Chryaene - K"pb) 5 85 91 6I-110 6 T BenaaWfluvzenNene ;WL(ppb) 5 92 98 49.146 7 BanScrmO:)Buoavebeve WA,(ppb) 5 N 9'a N-12D 8 B dmvp(Ipyaee pgh(ppb) 5a 89 It 58.126 7 Diteno(1.2,3<tl)traev.en 11(ppb) 10 100 67-IM 6 Dibenm(aL)enthacme ygro,(ppb) 5 100 106 67120 8 'Benm(g,M1.OPerylene pglL fppb) 5 92 9B 67I06 7 10 - Ytc �s;