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APPENDIX E: <br /> ANALYTICAL METHODS AND LABORATORY REPORTS <br /> Soil samples were analyzed for the following Historical Pipeline Portfolio—Bakersfield to <br /> Richmond(HPP-BTR) constituents, using methods contained in United States Environmental <br /> Protection Agency(EPA)publication SW-8461: <br /> • Total petroleum hydrocarbons quantified as crude oil (TPHc)by EPA Method 8015 <br /> Modified(CIO to C36); <br /> • Benzene, toluene, ethylbenzene, and total xylenes (BTEX)by EPA Method 8260B; and <br /> • Polynuclear aromatic hydrocarbons (PAHs)by EPA Method 8270 using selective ion <br /> monitoring. <br /> Groundwater samples were analyzed for the following HPP-BTR constituents,using methods <br /> contained in EPA publication SW-846: <br /> • TPH quantified as diesel (TPHd)by EPA Method 8015B Modified(C1O to C25). Silica- <br /> gel cleanup was performed on sample extracts that exceeded the laboratory reporting <br /> limit; <br /> • BTEX by EPA Method 8260B (using a 25-milliliter purge to attain HPP-BTR Risk <br /> Assessment Detection Limits); <br /> • PAHs by EPA Method 8270C (using large-volume injection to attain HPP-BTR Risk <br /> Assessment Detection Limits); and <br /> • General Minerals: Total dissolved solids (TDS)by EPA Method 160.1; sulfate, chloride, <br /> nitrate (as nitrogen), and nitrite (as nitrogen)by EPA 300.0; specific conductance by EPA <br /> 120.1; Kjeldahl nitrogen by EPA 351.2; total phosphorus by EPA 365.1; ammonia(as <br /> nitrogen)by 350.2; alkalinity(as calcium carbonate [CaC031), bicarbonate (as CaCO3), <br /> carbonate (as CaCO3), and hardness (as CaCO3)by SM 20 2320B; and boron, sodium, <br /> calcium, iron, magnesium, manganese, and potassium by SW846 6010B. <br /> QUALITY ASSURANCE PROCEDURES <br /> Quality assurance (QA) samples were collected to verify that no outside sources of <br /> contamination affected the groundwater samples. Laboratory-provided deionized water was <br /> decanted: <br /> • Directly from the deionized water container into laboratory-provided sample containers <br /> (QA-Field); <br /> • Through the plastic tubing used in sampling and into laboratory-provided sample <br /> containers (QA-Tubing); and <br /> • Through the clean pre-pack well screen and into laboratory-provided sample containers <br /> (QA-Screen). <br /> 1. EPA,2008. Test Methods for Evaluating Solid Waste,Physical/Chemical Methods. Update IV of the Third Edition. January. <br /> E-1 She Benham Companies,LLC <br /> AmmfjwU%�w AWholly Owned5uhsidiary <br /> From&&erne ro Sa ulruns <br />