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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425-717-656-2300 Fax:717-656-2681•www.larcasterIabs.com <br /> Page 1 of 4 <br /> REVISED <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgt. Co. Group Number: 1105583 <br /> Reported: 09/04/08 at 01:58 PM <br /> Matrix QC may not be reported if site-specific QC samples were not <br /> submitted. In these situations, to demonstrate precision and accuracy at <br /> a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br /> method. <br /> Laboratory Compliance Quality Control <br /> Blank Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL** Loo Units %REC %REC Limits RPD RPD Max <br /> Batch number: 08231SLGO26 Sample number(s) : 5442219-5442229 <br /> Naphthalene ND 0.00067 0.0017 mg/kg 71 67-105 <br /> Acenaphthylene ND 0.00033 0.0017 mg/kg 73 67-100 <br /> Acenaphthene ND 0.00067 0.0017 mg/kg 76 73-104 <br /> Fluorene ND 0.00067 0.0017 mg/kg 82 75-110 <br /> Phenanthrene ND 0.00067 0.0017 mg/kg 81 76-109 <br /> Anthracene ND 0.00033 0.0017 mg/kg 70 70-103 <br /> Fluoranthene ND 0.00067 0.0017 mg/kg 86 78-114 <br /> Pyrene ND 0.00067 0.0017 mg/kg 79 69-116 <br /> Benzo(a)anthracene ND 0.00067 0.0017 mg/kg 80 74-112 <br /> Chrysene ND 0.00033 0.0017 mg/kg 85 79-111 <br /> Benzo(b)fluoranthene ND 0.00067 0.0017 mg/kg 100 70-125 <br /> Benzo(k)fluoranthene ND 0.00067 0.0017 mg/kg 97 72-124 <br /> Benzo(a)pyrene ND 0.00067 0.0017 mg/kg 86 70-109 <br /> Indeno(1,2,3-cd)pyrene ND 0.00067 0.0017 mg/kg 101 64-127 <br /> Dibenz(a,h)anthracene ND 0.00067 0.0017 mg/kg 103 63-138 <br /> Benzo(g,h,i)perylene ND 0.00067 0.0017 mg/kg 97 58-131 <br /> Batch number: 082330007A Sample number(s) : 5442219-5442229 <br /> Total TPH ND 4.0 12 mg/kg 83 66-113 <br /> Batch number: B082311AA Sample number(s) : 5442219-5442221,5442224-5442226,5442228-5442229 <br /> Benzene ND 0.0005 0.005 mg/kg 96 99 84-115 3 30 <br /> Toluene ND 0.001 0.005 mg/kg 94 98 81-116 3 30 <br /> Ethylbenzene ND 0.001 0.005 mg/kg 94 98 82-115 4 30 <br /> Xylene (Total) ND 0.001 0.005 mg/kg 94 97 82-117 4 30 <br /> Batch number: R082311AB Sample number(s) : 5442222-5442223,5442227 <br /> Benzene ND 0.025 0.25 mg/kg 96 96 84-115 1 30 <br /> Toluene ND 0.050 0.25 mg/kg 98 98 81-116 0 30 <br /> Ethylbenzene ND 0.050 0.25 mg/kg 99 98 82-115 1 30 <br /> Xylene (Total) ND 0.050 0.25 mg/kg 98 98 82-117 0 30 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 08231SLGO26 Sample number(s) : 5442219-5442229 UNSPK: 5442222 <br /> Naphthalene -32677 -16813 27-145 14 30 <br /> (2) (2) <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />