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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425-717-656-2300 Fax:717-656-2681•www.larcasterIabs.com <br /> Page 1 of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgt. Co. Group Number: 1122196 <br /> Reported: 12/12/08 at 01:38 PM <br /> Matrix QC may not be reported if site-specific QC samples were not <br /> submitted. In these situations, to demonstrate precision and accuracy at <br /> a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br /> method. <br /> Laboratory Compliance Quality Control <br /> Blank Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL** Loo Units %REC %REC Limits RPD RPD Max <br /> Batch number: 083380010A Sample number(s) : 5542386-5542390 <br /> Total TPH N.D. 4.0 12 mg/kg 94 66-113 <br /> Batch number: 08338SLB026 Sample number(s) : 5542386-5542390 <br /> Naphthalene 0.0011 0.00067 0.0017 mg/kg 81 67-105 <br /> Acenaphthylene N.D. 0.00033 0.0017 mg/kg 85 67-100 <br /> Acenaphthene N.D. 0.00067 0.0017 mg/kg 84 73-104 <br /> Fluorene N.D. 0.00067 0.0017 mg/kg 90 75-110 <br /> Phenanthrene N.D. 0.00067 0.0017 mg/kg 92 76-109 <br /> Anthracene N.D. 0.00033 0.0017 mg/kg 87 70-103 <br /> Fluoranthene N.D. 0.00067 0.0017 mg/kg 91 78-114 <br /> Pyrene N.D. 0.00067 0.0017 mg/kg 83 69-116 <br /> Benzo(a)anthracene N.D. 0.00067 0.0017 mg/kg 88 74-112 <br /> Chrysene N.D. 0.00033 0.0017 mg/kg 89 79-111 <br /> Benzo(b)fluoranthene N.D. 0.00067 0.0017 mg/kg 89 70-125 <br /> Benzo(k)fluoranthene N.D. 0.00067 0.0017 mg/kg 90 72-124 <br /> Benzo(a)pyrene N.D. 0.00067 0.0017 mg/kg 80 70-109 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.00067 0.0017 mg/kg 92 64-127 <br /> Dibenz(a,h)anthracene N.D. 0.00067 0.0017 mg/kg 96 63-138 <br /> Benzo(g,h,i)perylene N.D. 0.00067 0.0017 mg/kg 88 58-131 <br /> Batch number: A083391AA Sample number(s) : 5542386-5542390 <br /> Benzene N.D. 0.0005 0.005 mg/kg 112 109 84-115 2 30 <br /> Toluene N.D. 0.001 0.005 mg/kg 106 105 81-116 2 30 <br /> Ethylbenzene N.D. 0.001 0.005 mg/kg 104 102 82-115 2 30 <br /> Xylene (Total) N.D. 0.001 0.005 mg/kg 104 104 82-117 1 30 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: 083380010A Sample number(s) : 5542386-5542390 UNSPK: 5542387 <br /> Total TPH 92 91 49-123 1 20 <br /> Batch number: 08338SLB026 Sample number(s) : 5542386-5542390 UNSPK: 5542387 <br /> Naphthalene 67 81 27-145 19 30 <br /> Acenaphthylene 51 61 42-141 18 30 <br /> Acenaphthene 73 85 37-145 14 30 <br /> Fluorene 78 90 51-142 14 30 <br /> Phenanthrene 77 90 42-144 14 30 <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />