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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike,PO Box 12425,Lancaster,PA 17605-2425-717-656-2300 Fax:717-656-2681•www.larcasterIabs.com <br /> Page 1 of 3 <br /> Quality Control Summary <br /> Client Name: Chevron Environmental Mgt. Co. Group Number: 1135073 <br /> Reported: 03/17/09 at 10:32 AM <br /> Matrix QC may not be reported if site-specific QC samples were not <br /> submitted. In these situations, to demonstrate precision and accuracy at <br /> a batch level, a LCS/LCSD was performed, unless otherwise specified in the <br /> method. <br /> Laboratory Compliance Quality Control <br /> Blank Blank Blank Report LCS LCSD LCS/LCSD <br /> Analysis Name Result MDL** Loo Units %REC %REC Limits RPD RPD Max <br /> Batch number: 090680019A Sample number(s) : 5616378-5616385 <br /> Total TPH N.D. 4.0 12 mg/kg 94 94 66-113 0 20 <br /> C10-C36 N.D. 4.0 12 mg/kg <br /> Batch number: 09068SLB026 Sample number(s) : 5616378-5616385 <br /> Naphthalene N.D. 0.00067 0.0017 mg/kg 84 84 67-105 0 30 <br /> Acenaphthylene N.D. 0.00033 0.0017 mg/kg 92 91 67-100 1 30 <br /> Acenaphthene N.D. 0.00067 0.0017 mg/kg 88 88 59-102 0 30 <br /> Fluorene N.D. 0.00067 0.0017 mg/kg 94 94 75-110 0 30 <br /> Phenanthrene N.D. 0.00067 0.0017 mg/kg 94 93 76-109 0 30 <br /> Anthracene N.D. 0.00033 0.0017 mg/kg 85 84 53-105 1 30 <br /> Fluoranthene N.D. 0.00067 0.0017 mg/kg 93 94 78-114 0 30 <br /> Pyrene N.D. 0.00067 0.0017 mg/kg 93 92 69-116 2 30 <br /> Benzo(a)anthracene N.D. 0.00067 0.0017 mg/kg 89 88 74-112 1 30 <br /> Chrysene N.D. 0.00033 0.0017 mg/kg 92 92 79-111 0 30 <br /> Benzo(b)fluoranthene N.D. 0.00067 0.0017 mg/kg 106 113 70-125 7 30 <br /> Benzo(k)fluoranthene N.D. 0.00067 0.0017 mg/kg 100 103 72-124 3 30 <br /> Benzo(a)pyrene N.D. 0.00067 0.0017 mg/kg 94 95 70-109 1 30 <br /> Indeno(1,2,3-cd)pyrene N.D. 0.00067 0.0017 mg/kg 107 111 47-140 4 30 <br /> Dibenz(a,h)anthracene N.D. 0.00067 0.0017 mg/kg 109 114 49-140 4 30 <br /> Benzo(g,h,i)perylene N.D. 0.00067 0.0017 mg/kg 103 107 44-138 3 30 <br /> Batch number: A090701AA Sample number(s) : 5616378-5616385 <br /> Benzene N.D. 0.0005 0.005 mg/kg 101 95 83-116 6 30 <br /> Toluene N.D. 0.001 0.005 mg/kg 98 92 81-112 7 30 <br /> Ethylbenzene N.D. 0.001 0.005 mg/kg 98 92 79-110 7 30 <br /> Xylene (Total) N.D. 0.001 0.005 mg/kg 99 93 78-108 7 30 <br /> Sample Matrix Quality Control <br /> Unspiked (UNSPK) = the sample used in conjunction with the matrix spike <br /> Background (BKG) = the sample used in conjunction with the duplicate <br /> MS MSD MS/MSD RPD BKG DUP DUP Dup RPD <br /> Analysis Name %REC %REC Limits RPD MAX Conc Conc RPD Max <br /> Batch number: A090701AA Sample number(s) : 5616378-5616385 UNSPK: P615277 <br /> Benzene 101 55-143 <br /> Toluene 97 50-146 <br /> Ethylbenzene 97 44-141 <br /> Xylene (Total) 96 44-136 <br /> *-Outside of specification <br /> **-This limit was used in the evaluation of the final result for the blank <br /> (1)The result for one or both determinations was less than five times the LOQ. <br /> (2)The unspiked result was more than four times the spike added. <br />