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FRIEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For PNA Compounds By EPA Method 8270C SIM <br /> Client Sample ID: GMX-8-5.0 Client: Geomatrix Consultants, Inc. <br /> Date Received: 05/23/02 Project: 6447.001 (US Can) <br /> Date Extracted: 06/03/02 Lab ID: 205181-011/10 <br /> Date Analyzed: 06/06/02 Data File: 060529.D <br /> Matrix: Soil Instrument: GCMS3 <br /> Units: ug/kg (ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: % Recovery Limit Limit <br /> Anthracene-d10 115 vo 43 109 <br /> Benzo(a)anthracene-d12 64 vo 65 134 I <br /> Concentration: <br /> Compounds: ug/kg (ppb) E <br /> Naphthalene <250 {f <br /> Acenaphthylene <250 <br /> Acenaphthene <250 f <br /> Fluorene <250 J{ <br /> Phenanthrene <250 <br /> Anthracene X250 <br /> Fluoranthene <250 <br /> Pyrene <250 <br /> Benz(a)anthracene <250 <br /> Chrysene <250 ' <br /> Benzo(b)fluoranthene <250 <br /> Ben zo(k)fluoran th ene <250 I <br /> Benzo(a)pyrene <250 <br /> Indeno(1,2,3-cd)pyrene <250 i <br /> Dibenzo(a,h)anthracene <250 , <br /> Benzo(g,h,i)perylene X250 <br /> Note: The sample was diluted due to high levels of interfering compounds. Detection limits are raised <br /> due to dilution and surrogate recoveries may not be meaningful. <br /> vo-The value reported fell outside the control limits established for this analyte. <br /> 7 <br />