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FRIEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Analysis For PNA Compounds By EPA Method 8270C STM <br /> Client Sample ID: GMX-113-30.0 Client: Geomatrix Consultants, Inc. <br /> Date Received: 05/23/02 Project: 6447.001 (US Can) <br /> Date Extracted: 06/03/02 Lab ID: 205181-12 1110 <br /> Date Analyzed: 06/05/02 Data File: 060525.1) <br /> Matrix: Soil Instrument: GCMS3 <br /> Units! ug/kg (ppb) Operator: YA <br /> Lower Upper <br /> Surrogates: % Recovery Limit Limit <br /> Anthracene-d10 90 43 109 <br /> Benzo(a)anthracene-d12 109 65 134 <br /> Concentration: <br /> Compounds: ug/kg (ppb) <br /> Naphthalene X50 <br /> Acenaphthylene <50 ,.` <br /> Acenaphthene 240 <br /> Fluoren e 610 <br /> Phenanthrene 470 <br /> Anthracene <50 <br /> Fluoranthene X50 <br /> Pyrene 82 <br /> Benz(a)anthracene X50 <br /> Chrysene 160 <br /> Benzo(b)flu oran then e X50 <br /> Benzo(k)fluoranthene X50 <br /> Benzo(a)pyrene <50 <br /> Indeno(1,2,3-ed)pyrene <50 <br /> Dibenzo(a,h)anthracene X50 <br /> Benzo(g,h,i)perylene <50 <br /> Note: The sample was diluted due to high levels of interfering compounds. Detection limits are raised <br /> due to dilution and surrogate recoveries may not be meaningful. <br /> 18 <br />