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FRIEDMAN & BRUYA, INC. <br /> ENVIRONMENTAL CHEMISTS <br /> Date of Report: 08/18/03 <br /> Date Received: 08/06103 <br /> Project: 6447.001 ([U.S. CAN), F&BI 308040 <br /> QUALITY ASSURANCE RESULTS FOR THE ANALYSIS OF WATER. <br /> SAMPLES FOR. PNXS BY EPA. METHOD 8270C SIM <br /> Laboratory Code: Laboratory Control Sample <br /> Percent Percent <br /> Reporting Spike Recovery Recovery Acceptance RPD <br /> Analyte Units Level LCS LCSD Criteria (Limit 20) <br /> Naphthalene µglL (ppb) 5 90 92 62-128 3 <br /> Acenaphthylene µg/L (ppb) 5 96 98 67-140 3 <br /> Acenaphthene: µglL (ppb) 5 97 100 62-132 4 <br /> Fluorene µg/l, (ppb) 5 94 98 66-137 4 <br /> Phenanthrene µg1L (ppb) 5 93 97 59-133 5 <br /> Anthracene µg/L (ppb) 5 87 90 64-145 4 <br /> Fluoranthene µg/l, (ppb) 5 91 94 65.139 3 <br /> Pyrene µglL (ppb) 5 94 96 64-140 3 <br /> Benz(a)anthracene µglL (ppb) 5 92 95 57-135 3 <br /> Chrysene µg/l, (ppb) 5 82 85 57-125 4 <br /> Benzo(b)lluoranthenc yLglL (ppb) 5 124 129 47-149 4 <br /> Benzo(k)fluoranthene ug/L (ppb) 5 91 93 46-139 3 <br /> Benzo(a)pyrene µglL (ppb) 5 99 102 57-143 3 <br /> 1ndeno(1,2,3-cd)pyreno �LgIL (ppb) 5 90 93 58-147 3 <br /> Dibenzo(a,h)anthracene µg/l, (ppb) 5 94 98 56-152 4 <br /> Benzo(g,hJ)perylene µg/L (ppb) 5 88 92 53-146 4 <br /> 16 <br />