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ParameterValueUnits Method AnalyzedProject Name :Project Number :Parcel 2A211602193.400.400Report Number : 80104Date : 01/25/2012SpikedSampleSample Spike LevelSpikeDup.LevelSpiked SampleValueSpiked SampleValueDuplicatePercent Spiked SampleRecov.Percent Spiked SampleRecov.DuplicateRelativePercentDiff.Percent Spiked SampleRecov.LimitRelativePercentDiff.LimitAnalysis DateQC Report : Matrix Spike/ Matrix Spike DuplicateBLANKTPH as Diesel<50 ug/L M EPA 8015 1/20/121000 1000 1030 964 103 96.4 6.76 70-130 2580104-01Benzene<0.50 ug/L EPA 8260B 1/19/1240.0 40.0 38.1 36.6 95.3 91.6 3.88 80-120 2580104-01Diisopropyl ether<0.50 ug/L EPA 8260B 1/19/1239.5 39.5 41.3 41.5 104 105 0.612 80-120 2580104-01Ethyl-tert-butyl ether<0.50 ug/L EPA 8260B 1/19/1240.0 40.0 42.0 42.0 105 105 0.197 76.5-120 2580104-01Ethylbenzene<0.50 ug/L EPA 8260B 1/19/1240.0 40.0 41.3 38.8 103 97.0 6.20 80-120 2580104-01Methyl-t-butyl ether<0.50 ug/L EPA 8260B 1/19/1240.4 40.4 44.1 44.4 109 110 0.769 69.7-121 2580104-01P + M Xylene<0.50 ug/L EPA 8260B 1/19/1240.0 40.0 41.7 39.4 104 98.5 5.61 76.8-120 2580104-01Tert-Butanol<5.0 ug/L EPA 8260B 1/19/12201 201 197 198 97.8 98.6 0.806 80-120 2580104-01Tert-amyl-methyl ether<0.50 ug/L EPA 8260B 1/19/1239.4 39.4 40.9 41.4 104 105 1.05 78.9-120 252795 2nd Street, Suite 300 Davis, CA 95618 530-297-4800KIFF ANALYTICAL, LLCPage 22 of 35