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110 Second Avenue South,#D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC. Telephone:925-798-1620 Fax:925-798-1622 <br /> htW://w%vw.mccampbell.com E-mail:main@mccampbell.com <br /> Advanced GeoEnviromnental Client Project ID:Waterloo Food&Fuel Date Sampled: 02/22/99 <br /> 4005 North Wilson Way Date Received. 02/23/99 <br /> Client Contact: Bob Marty Date Extracted: 02/23/99 <br /> Stockton, CA 95205 I <br /> Client P.O: Date Analyzed: 02/23/99 <br /> Lead* <br /> EPA analytical methods 60101200.7,239.2' <br /> Lab ID Client ID Matrix .Extraction° Lead* %Recovery <br /> Surrogate <br /> 03762 TS-1-14 S TTLC 6.4 100 <br /> 03763 TS-2-14 S TTLC 6.7 103 <br /> 03764 TS-3-14 S TTLC 6.5 100 <br /> 03763 TS-4-14 S TTLC 7.6 102 <br /> S TTLC 3.0 mg/kg <br /> Reporting Limit unless otherwise <br /> stated;ND means not detected above W TTLC 0.005 mg/L <br /> the reporting limit <br /> STLC,TCLP 0.2 mg/L <br /> *soil and sludge samples are reported in mg,kg,wipe samples in ug/wipe,and.eater samples and all STLC I SPLP I TCLP extracts in mg/L <br /> 'Lead is analysed using .EPA method 6010 (ICP)for soils, sludges, STLC & TCLP extracts and method 239.2 (AA Furnace) for water <br /> samples <br /> °EPA extraction methods 1311(TCLP),3010/3020(water,TfLC),3040(organic matrices,TTLC),3050(solids,TTLC);STLC-CA Title 22 <br /> °surrogate diluted out of range,N/A means surrogate not applicable to this analysis <br /> reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than --2 vol. % sediment; this sediment is extracted with the liquid, in accordance with EPA <br /> methodologies and can significantly effect reported metal concentrations. <br /> DHS Certification No. 1644 /�/ Edward Hamilton,Lab Director <br />