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* MICROBAc° <br /> Microbac Laboratories Inc., - Marietta, OH <br /> CERTIFICATE OF ANALYSIS <br /> MlJ0460 <br /> Client Sample ID: Fedex CA-1-2 <br /> Sample Matrix: Sotid <br /> Lab Sample ID: MlJ0460-01 Collection Date: 10/0512021 12:00 <br /> Volatile Organic Compounds by Result RL Units DF Note Prepared Analyzed Analyst <br /> GCMS <br /> Surrogate:1,2-Dlchloroethane-d4 85.3 Limit:80-120 %Rec 1 10108/21 1339 10108121 2221 JDS <br /> Surrogate:Toluene-d8 101 Limit:81-117 %Rec 1 10/08/21 1339 10108121 2221 JDS <br /> Extractable Hydrocarbons by GC/FID Result RL Units OF Note Prepared Analyzed Analyst <br /> EPA 3550BIEPA 8015D <br /> Diesel Range Organics(C10-C28) x14000 14000 uglkg dry 1 10112121 1340 10/13121 2031 KJB <br /> Oil Range Organics(C28-C40) <69800 69800 uglkg dry 1 10112121 1340 10/13121 2031 KJB <br /> Surrogate:o-Terphenyl 63.0 Limit:43-136 %Rec 1 10112121 1340 10/13121 2031 KJB <br /> Surrogate:Octacosano 89.9 Limit:25-162 %Rec 1 10/12121 1340 10/13/21 2031 KJB <br /> Definitions <br /> %(by wt.): Percent by Weight <br /> 02: LCS recovery is above acceptance limits.However there is no impact on the reported value. <br /> Q4: ICV recovery is above acceptance limits.The reported value is estimated. <br /> Q7: CCV recovery is above acceptance limits.However there is no impact on the reported value. <br /> 08: CCV recovery is below acceptance limits.The reported value is estimated. <br /> RL: Reporting Limit <br /> uglkg: Micrograms per Killogram <br /> Cooler Receipt Log <br /> Cooler ID: Default Cooler Temp: 1.4°C <br /> Cooler Inspection Checklist <br /> Ice Present or not required? Yes Shipping containers sealed or not required? Yes <br /> Custody seals intact or not required? Yes Chain of Custody(COC)Present? Yes <br /> COC includes customer information? Yes Relinquished and received signature on COC? Yes <br /> Sample collector identified on COC? Yes Sample type identified on COC? Yes <br /> Correct type of Containers Received Yes Correct number of containers listed on COC? Yes <br /> Containers Intact? Yes COC includes requested analyses? Yes <br /> Enough sample volume for indicated tests received? Yes Sample labels match COC(Name,Date&Time?) No <br /> Samples arrived within hold time? Yes Correct preservatives on COC or not required? Yes <br /> Chemical preservations checked or not required? Yes Preservation checks meet method requirements? Yes <br /> VOA vials have zero headspace,or not recd.? Yes <br /> Report Comments Reviewed and Approved By: <br /> The data and information on this,and other accompanying documents,represents only the 'N <br /> sample(s)analyzed. This report is incomplete unless all pages indicated in the footnote are Alicia Walker <br /> present and an authorized signature is included. The services were provided under and Project Manager <br /> subject to Microbac's standard terms and conditions which can be located and Reported: 10/14/2021 15:30 <br /> reviewed at<https://www.microbac.com/standard-terms-conditions?. <br /> Microbac Laboratories, Inc. <br /> 158 Starlite Drive I Marietta,01-1145750 1800.373.4071 p I www.microbac.com <br />