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<br />CALIFORNIA LABORATORY SERVICES <br /> <br />Page 16 of 18 <br />Committed. Responsive. Flexible. <br /> <br />06/22/20 15:18 <br />PSC Industrial Outsourcing Project: McDonald Foland TOE Spill Turner Creek <br />5780 Obata Way Suite A. Project Number: 178-2001-00240472 CLS Work Order #: 20F0790 <br />Gilroy, CA 95020 <br /> <br />Project Manager: David Matthews COC #: 196111 <br />Volatile Organic Compounds by EPA Method 8260B - Quality Control <br />Analyte Result <br />Reporting <br />Limit Units <br />Spike Source <br />Level Result %REC <br />%REC <br />Limits RPD <br />RPD <br />Limit Notes <br />Batch 2004775 - EPA 5030 Soil MS <br />Blank (2004775-BLK1) Prepared & Analyzed: 06/18/20 <br />Vinyl chloride ND 10 rig/kg <br />Xylenes (total) ND 10 <br />Di-isopropyl ether ND 5.0 <br />Ethyl tert-butyl ether ND 5.0 <br />tert-Amyl methyl ether ND 5.0 <br />tert-Butyl alcohol ND 50 <br />Surrogate: 1,2-Dichloroethane-d4 29.9 30.0 100 50-125 <br />Surrogate: Toluene-d8 24.6 111 30.0 82 62-125 <br />Surrogate: 4-Bromoiluorobenzene 33.2 30.0 111 50-128 <br />LCS (2004775-BS1) Prepared & Analyzed: 06/18/20 <br />Benzene 21.9 5.0 vg/kg 20.0 109 64-135 <br />Chlorobenzene 23.0 5.0 20.0 115 67-133 <br />1,1-Dichloroethene 18.5 5.0 20.0 93 53-137 <br />Toluene 21.1 5.0 20.0 106 61-138 <br />Trichloroethene 19.2 5.0 20.0 96 64-130 <br />Surrogate: 1,2-Dich1oroethane-d4 26.1 30.0 87 50-125 <br />Surrogate: Toluene-d8 29.3 30.0 98 62-125 <br />Surrogate: 4-Bromoiluorobenzene 25.5 30.0 85 50-128 <br />LCS Dup (2004775-BSD1) Prepared & Analyzed: 06/18/20 <br />Benzene 20.9 5.0 gek8 20.0 105 64-135 4 30 <br />Chlorobenzene 21.0 5.0 20.0 105 67-133 9 30 <br />1,1-Dichloroethene 23.4 5.0 20.0 117 53-137 23 30 <br />Toluene 21.5 5.0 20.0 108 61-138 2 30 <br />Trichloroethene 20.9 5.0 20.0 105 64-130 9 30 <br />Surrogate: 1,2-Dichloroethane-d4 27.7 30.0 92 50-125 <br />Surrogate: Toluene-d8 29.7 30.0 99 62-125 <br />Surrogate: 4-Bromofluorobenzene 25.0 30.0 83 50-128 <br />3249 Fitzgerald Road, Rancho Cordova, CA 95742 I 800.638.7301 I Tel: 916.638.7301 x102 I Fax: 916.638.4510 I www.californialab.com <br />Small Business #2916 I ELAP #1233 I NAICS #541380 I CA SWRCB ELAP Accreditation/Registration Number 1233