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E3=mma-K <br />ASSOCIATES <br />BSKAssociates Laboratory Fresno <br />A7C1878 <br />Genera/ <br />EPA 8260B - Quality Control <br />Batch: A703742 <br />Prep Method: no prep -volatiles <br />Blank (A703742-BLK1) <br />Prepared: 3/24/2017 <br />Analyst: AMN <br />1,2-Dibromoethane (EDB) <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />1,2-Dichloroethane <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Benzene <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Di -isopropyl ether (DIPE) <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Ethyl tort -Butyl Ether (ETBE) <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Ethylbenzene <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />m,p-Xylenes <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Methyl -t -butyl ether <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Naphthalene <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />o -Xylene <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />tert-Amyl Methyl Ether (TAME) <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />tert-Butyl alcohol (TBA) <br />ND <br />50 <br />ug/kg <br />03/24/17 <br />Toluene <br />ND <br />5.0 <br />ug/kg <br />03/24/17 <br />Surrogate: 1,2-Dichloroethane-d4 <br />51 <br />ug/kg <br />50 <br />102 70-130 03/24/17 <br />Surrogate: Bromotluorobenzene <br />55 <br />o -Xylene <br />50 <br />111 70-130 03/24/17 <br />Surrogate: Toluene -d8 <br />51 <br />106 <br />50 <br />102 70-130 03/24/17 <br />Blank Spike (A703742 -BSI) <br />1,2-Dibromoethane (EDB) <br />22 <br />5.0 <br />ug/kg <br />20 <br />109 <br />65-135 <br />03/24/17 <br />1,2-Dichloroethane <br />20 <br />5.0 <br />ug/kg <br />20 <br />100 <br />81-146 <br />03/24/17 <br />Benzene <br />19 <br />5.0 <br />ug/kg <br />20 <br />97 <br />75-147 <br />03/24/17 <br />Di -isopropyl ether (DIPE) <br />21 <br />5.0 <br />ug/kg <br />20 <br />103 <br />80-126 <br />03/24/17 <br />Ethyl tert-Butyl Ether (ETBE) <br />21 <br />5.0 <br />ug/kg <br />20 <br />105 <br />84-126 <br />03/24/17 <br />Ethylbenzene <br />21 <br />5.0 <br />ug/kg <br />20 <br />107 <br />75-123 <br />03/24/17 <br />m,p-Xylenes <br />39 <br />5.0 <br />ug/kg <br />40 <br />99 <br />75-118 <br />03/24/17 <br />Methyl -t -butyl ether <br />40 <br />5.0 <br />ug/kg <br />40 <br />100 <br />73-147 <br />03/24/17 <br />Naphthalene <br />20 <br />5.0 <br />ug/kg <br />20 <br />98 <br />37-169 <br />03/24/17 <br />o -Xylene <br />21 <br />5.0 <br />ug/kg <br />20 <br />106 <br />73-121 <br />03/24/17 <br />tert-Amyl Methyl Ether (TAME) <br />20 <br />5.0 <br />ug/kg <br />20 <br />99 <br />79-129 <br />03/24/17 <br />tort -Butyl alcohol (TBA) <br />210 <br />50 <br />ug/kg <br />200 <br />103 <br />72-130 <br />03/24/17 <br />Toluene <br />21 <br />5.0 <br />ug/kg <br />20 <br />107 <br />65-136 <br />03/24/17 <br />Surrogate:l,2-Dichloroethane-d4 <br />50 <br />50 <br />99 <br />70-130 <br />03/24/17 <br />Surrogate: Bromofluorobenzene <br />51 <br />50 <br />102 <br />70-130 <br />03/24/17 <br />Surrogate: Toluene -d8 <br />51 <br />50 <br />102 <br />70-130 <br />03/24/17 <br />Blank Spike Dup (A703742-BSD1) <br />1,2-Dibromoethane (EDB) <br />21 <br />5.0 ug/kg 20 <br />106 <br />65-135 <br />3 <br />30 <br />03/24/17 <br />1,2-Dichloroethane <br />21 <br />5.0 ug/kg 20 <br />105 <br />81-146 <br />5 <br />30 <br />03/24/17 <br />Benzene <br />20 <br />5.0 ug/kg 20 <br />99 <br />75-147 <br />2 <br />30 <br />03/24/17 <br />Di -isopropyl ether (DIPE) <br />19 <br />5.0 ug/kg 20 <br />94 <br />80-126 <br />10 <br />30 <br />03/24/17 <br />Ethyl tert-Butyl Ether (ETBE) <br />18 <br />5.0 ug/kg 20 <br />90 <br />84-126 <br />15 <br />30 <br />03/24/17 <br />Ethylbenzene <br />21 <br />5.0 ug/kg 20 <br />104 <br />75-123 <br />3 <br />30 <br />03/24/17 <br />m,p-Xylenes <br />39 <br />5.0 ug/kg 40 <br />98 <br />75-118 <br />1 <br />30 <br />03/24/17 <br />Methyl -t -butyl ether <br />36 <br />5.0 ug/kg 40 <br />90 <br />73-147 <br />10 <br />30 <br />03/24/17 <br />Naphthalene <br />19 <br />5.0 ug/kg 20 <br />97 <br />37-169 <br />1 <br />30 <br />03/24/17 <br />o -Xylene <br />21 <br />5.0 ug/kg 20 <br />103 <br />73-121 <br />3 <br />30 <br />03/24/17 <br />A7C1878 FINAL 05022017 1255 <br />Printed: 5/2/2017 <br />'Amended Report *** <br />Page 4 of 9 <br />QA -RP -0001-10 Final.rpt <br />www.BSKAssociates.com <br />