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/-1-I McCampbell Analytical, Inc. <br />czw4e "When Quality Counts" <br />1534 Willow Pass Road, Pittsburg, CA 94565-1701 <br />Toll Free Telephone: (877) 252-9262 / Fax: (925) 252-9269 <br />http://www.mccampbell.com / E-mail: main@mecampbell.com <br /> <br />Quality Control Report <br />Client: Yara North America <br />Date Prepared: 01/14/2021 <br />Date Analyzed: 01/14/2021 <br />Instrument: GC45 <br />Matrix: Soil <br />Project: New Site Pond <br />WorkOrder: 2101638 <br />BatchID: 213160 <br />Extraction Method: SW5030B <br />Analytical Method: SW8260B <br />Unit: mg/kg <br />Sample ID: MB/LCS/LCSD-213160 <br />QC Summary Report for SW8260B <br />Analyte MB <br />Result <br />MDL RL SPK <br />Val <br />MB SS <br />%REC <br />MB SS <br />Limits <br />cis-1,3-Dichloropropene 0.000778,J 0.000660 0.00500 <br />trans-1,3-Dichloropropene 0.00170,J 0.000670 0.00500 <br />Diisopropyl ether (DIPE) ND 0.000780 0.00500 <br />Ethylbenzene ND 0.00110 0.00500 <br />Ethyl tert-butyl ether (ETBE) ND 0.000730 0.00500 <br />Freon 113 ND 0.00110 0.00500 <br />Hexachlorobutadiene ND 0.00120 0.00500 <br />Hexachloroethane ND 0.000670 0.00500 <br />2-Hexanone ND 0.00430 0.00500 <br />lsopropylbenzene ND 0.00140 0.00500 <br />4-Isopropyl toluene ND 0.00130 0.00500 <br />Methyl-t-butyl ether (MTBE) ND 0.00140 0.00500 <br />Methylene chloride ND 0.00580 0.0200 <br />4-Methyl-2-pentanone (MIBK) ND 0.00150 0.00500 <br />Naphthalene ND 0.00220 0.00500 <br />n-Propyl benzene ND 0.00160 0.00500 <br />Styrene ND 0.00120 0.00500 <br />1,1,1,2-Tetrachloroethane ND 0.00100 0.00500 <br />1,1,2,2-Tetrachloroethane ND 0.000280 0.00500 <br />Tetrachloroethene ND 0.000310 0.00500 <br />Toluene 0.00130,J 0.00120 0.00500 <br />1,2,3-Trichlorobenzene ND 0.00170 0.00500 <br />1,2,4-Trichlorobenzene ND 0.00120 0.00500 <br />1,1,1-Trichloroethane ND 0.000840 0.00500 <br />1,1,2-Trichloroethane ND 0.000920 0.00500 <br />Trichloroethene ND 0.000810 0.00500 <br />Trichlorofluoromethane ND 0.00130 0.00500 <br />1,2,3-Trichloropropane ND 0.000150 0.00500 <br />1,2,4-Trimethylbenzene ND 0.00320 0.00500 <br />1,3,5-Trimethylbenzene ND 0.00120 0.00500 <br />Vinyl Chloride ND 0.000130 0.00500 <br />m,p-Xylene ND 0.00250 0.00500 <br />o-Xylene ND 0.00120 0.00500 <br />(Cont.) <br />CA ELAP 1644 • NELAP 40330RELAP <br />Page 34 of 51